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110 2nd Avenue South #D7,Pacheco,CA 94553 5560 <br /> McCampbell Analytical, Inc. Telephone 925 798-1620 Fax 925 798 1522 <br /> ) Website www mccampkell coin E-mail main mccampbell coin <br /> Advanced GeoEnvironmental, Inc Client Project ID Stockton Plat-Feb GW Datc Sampled 02/11/04 <br /> . 837 Shaw Road Date Received 02/12/04 <br /> Client Contact Bill Little Date Extracted 02/12/04 <br /> Stockton,CA 95215 Client P O Date Analyzed 02/18/04 <br /> Seinivolatiles Organics by GC/MS(625 Basic Target List)* <br /> Extracoen Method SW3535A Analytical Method SW8270D Work Order 0402163 <br /> Lab ID 0402163-OOIF <br /> Client ID Effluent <br /> Matrix Water <br /> portmCompound Concentration* DF R` ,,,ni a Compound Concentration* DF RiUtmi s <br /> Acenaphthene ND<20 20 1 0 Acena hth lene ND<200 20 10 <br /> Anthracene ND<200 20 10 Benzidine ND<100 20 50 <br /> Ben7o(a anthracene ND<200 20 10 Benzo(b)tluoranthene ND<200 20 10 <br /> Benzo k fluoranthene ND<200 20 10 Benzo( h,t) lene ND<100 20 50 <br /> Benzo(a)pyrene ND<200 20 10 Bis(2-chloroethox Methane ND<100 20 50 <br /> Bis(2-chloroeth l)Ether ND<20 20 10 Bis 2-chlorotso ropyl)Ether ND<40 20 20 <br /> Bis(2-cth lhex t)Adipate ND<100 20 50 Bis(2-eth lhex 1)Phthalate ND<100 20 50 <br /> 4-BromO hen i Phen I Ether ND<100 20 50 Mu—tylbenzyl Phthalate 230 20 10 <br /> 4-Chloro-3-meth I henol ND<20 20 1 0 2-Chlorona hthalene ND<200 20 10 <br /> 2-Chloro henol ND<100 20 50 4-Chloro hen 1 Phen 1 Ether ND<100 20 50 <br /> Ch Bene ND<200 20 10 D:benzo a,h anthracene ND<200 20 10 <br /> Di-n-butyl Phthalate ND<200 20 10 1,2-Dichlorobenzene ND<40 20 20 <br /> 1,3-Dichlorobenzene ND<20 20 10 1,4-Dichlorobenzene ND<20 20 10 <br /> 3,3-Dichlorobenzidme ND<100 20 50 2 4-Dichloro henol ND<100 20 so <br /> Diethyl Phthalate ND<40 20 20 2,4-Dimeth I henol ND<40 20 20 <br /> Dimeth I Phthalate ND<40 20 20 4,6-Dimtro-2-meth I henol ND<100 20 —50 <br /> 2,4-Dinrtro henol ND<100 20 50 2,4-Dinitrotoluene ND<100 20 50 <br /> 2,6-Dinitrotoluene ND<100 20 50 Di-n-oct l Phthalate ND<200 20 10 <br /> 1,2-Di hen lh drazme ND<20 T 20 10 Fluoranthene ND<20 20 1 0 <br /> Fluorene N13<200 20 10 Hexachlorobenzene ND<20 20 10 <br /> Hexachlorobutadiene ND<20 20 10 Hexachloroc clo entadiene ND<100 20 50 <br /> Hexachlomethane ND<20 20 1 0 j Indeno 1,2,3-cd ene ND<200 20 10 <br /> Isa horone ND<20 20 10 Na hthalene ND<20 20 IT <br /> Nitrobenzene ND<20 20 10 2-Nitrophenol ND<200 20 10 <br /> 4-Nitrophenol ND<200 20 10 N-Nitrosodimeth lamine ND<30 20 50 <br /> N-Nitrosodi hen ]amine i ND<20 20 1 0 N-Nitrosodi-n-propylainine ND<100 20 50 <br /> Pentachlorophenol ND<100 20 5 0 Phenanthrenc ND<100 20 so <br /> Phenol ND<20 20 l0 Pyrene ND<200 20 10 <br /> 1 2 4-Tnehlorobenzene ND<100 20 1 5 0 2 4 6-Tnchloro henol I ND<200 1 20 10 <br /> _ Surrogate Recoveries(%) <br /> %SS --# %SS 570 <br /> %SS --# %SS ---# <br /> %SS 584 %SS ---# <br /> Comments <br /> *water samples and all TCLP&SPLA extracts are reported inµg/L,soil/sludge/soltd samples in mg/kg,wipe samples in jig/wipe,product/oil/non- <br /> aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> Lh)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> arae content <br /> DHS Certification No 1644 Angela Rydebus, Lab Manager <br />