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110 2nd Avenue South 4D7 Pacheco,CA 94553-5560 <br /> 4 1 McCarnpbell Analytical, Inc. Telephone 925-798-1620 Fax 925-798-1622 <br /> Website www mccampbell com E-mail roam@mmampbelt corn <br /> Advanced GeoEnvironmental,Inc Client Project ID Former SP-KE L Date Sampled 03/23/04 <br /> Business <br /> 837 Shaw Road Date Received 03/24/04 <br /> Stockton,CA 95215 Client Contact Bill Little Date Extracted 03/24/04 <br /> Client P O Date Analyzed 03/25/04 <br /> Seimvolatiles Organics by GC/MS (625 Basic Target List)* <br /> Extraction Method SW3535A Analytical Method SW8270D Work Order 0403387 <br /> Lab ID 0403387-OOIB <br /> LEI Client ID Effluent <br /> Matrix Water <br /> Compound Concentration* DF R „v g Compound Concentration * DF kwrtmg <br /> umt <br /> Acenaphthene ND 40 4 Acenaphthylene ND 40 40 <br /> Anthracene ND 40 40 Benzidine ND 40 20 <br /> Benzo(a)anthracene ND 40 40 Benzo(b)fluoranthene ND 40 40 <br /> Benzo(k)fluoranthene ND 40 40 Benzo(g,h,i)peiylene ND 40 20 <br /> Benzo(a)pyrene ND 40 40 Bis(2-chloroethoxy)Methane ND 40 20 <br /> Bis(2-chloroethyl)Ether ND 40 4 Bis(2-chloroisopropyl)Ether ND <br /> Bis(2-ethylhexyl)Adipate ND 40 20 Bis(2-ethylhexyl)Phthalate ND 40 i 20 <br /> 4-Bromophenyl Phenyl Ether ND 40 20 Butylbenzyl Phthalate ND 40 40 <br /> 4-Chloro-3-methylphenol ND 40 4 2-Chloronaphthalene ND 40 40 <br /> 2-Chlorophenol ND 40 20 4-Chlorophenyl Phenyl Ether ND 4 0 20 <br /> Chrysene ND 40 40 Dibenzo(a h)anthracene ND E 40 40 <br /> Di-n-butyl Phthalate ND 40 40 1 2-Dichlorobenzene ND 40 8 <br /> 1,3-Dichlorobenzene ND 40 4 1,4-Dichlorobenzene ND 40 4 <br /> 3 3-Dtchlorobenzidine ND 40 20 2,4-Dichlorophenol ND 40 20 <br /> Diethyl Phthalate ND 40 8 2,4-Dimethylphenol ND 40 8 <br /> Dimethyl Phthalate ND 40 8 4,6-Dimtro-2-methylphenol ND_ 4 0 20 <br /> 2,4-Dinitrophenol ND 40 20 2,4-Dinitrotoluene ND _ 40 20 <br /> 2,6-Dmitrotoluene ND 40 20 Di-n-octyl Phthalate ND _ 40 40 <br /> 1,2-Diphenylhydrazine ND 40 4 Fluoranthene ND 40 4 <br /> Fluorene ND 40 40 Hexachlorobenzene ND 40 4 <br /> liexachlorobutadiene ND 40 4 flexachlorocyclopentadiene ND 40 20 <br /> l-lexachloroethane ND 40 4 Indeno(I,2,3-cd)pyrene ND 40 40 <br /> Isophorone ND 40 4 Naphthalene ND 40 4 <br /> Nitrobenzene ND 40 4 2-Nitrophenol ND 40 40 <br /> 4-Nitrophenol ND 40 40 N-Nitrosodimethylamme ND 40 20 <br /> N-Nitrosodiphenylamine ND 40 4 N-Nitrosodi-n-propylamine ND 40 20 <br /> Pentachlorophenol ND 40 20 Phenanthrene ND 4 0 20 <br /> Phenol ND 40 4 Pyrene ND 40 40 <br /> 1 2,4-Trtchlorobenzene ND 40 20 2,44-Trichlorophenol ND 40 40 <br /> Surrogate Recoveries(%) <br /> %SS 767 %SS 785 <br /> %SS 782 %SS 887 <br /> %SS 825 %SS 66 1 <br /> Comments <br /> *water samples and all TCLP&SPLP extracts are reported in gg/L,soil/sludge/solid samples in mg(kg,wipe samples inµg/wipe,producttoil/non- <br /> aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> • #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> h)lighter than water immiscible shcen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 _ _Angela Rydehus, Lab Manager <br />