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,1 a1 <br /> -- --��— 110 2,1d1%%cn114 Sou1h 41)1 P«.hecu [ A 94N5+:060 <br /> Mccampbefi Analytical, Ince _ lelr.010116 92" 'vH IWO IdA 921- ))�f' 16_'1 <br /> \ketl,Ite MN SA nxc.ampixllc.um I nw,l uran,,nuxcan,ptwllc.nu III <br /> QC SUMMARY REPORT FOR SW8260B <br /> W O Sample Matrix Water QC Matrix Water Work0rder 0641215 <br /> EPA Method SW8260B Extraction SW5030B BatchlD 19884 Spiked Sample ID 0601212-001B <br /> Anal to Sample Spaked MS MSD MS-MSD LCS LCSD !LCS-LCSD Acceptance Criteria(%) <br /> Y -- — - <br /> pg/L pg/L % Rec %Rec %, RPD % Rec % Rec % RPD IVIS/MSD LCS/LCSD <br /> tail-Amyl nuthyl 1,ther(TIMI-) ND 10 119 119 0 109 109 0 70- 130 70- 130 <br /> t Butyl alcohol(I BA) ND 50 907 95 9 5 53 946 98 6 4 18 70-130 70-130 <br /> Dw;opropyl eche: (DIPE) ND 10 1 1 1 120 760 113 116 219 70- 130 70- 13C <br /> Ethyl lert-butyl tither(ETRE) ND 10 104 109 443 939 942 0 382 70-130 70-130 <br /> Methyl-t-butyl ether(M I]ih) ND 10 t00 100 � 0 88 7 91 3 286 70-130 70-130 <br /> "/SSI 103 to 102 100 230 100 100 0 70-130 70-130 <br /> All target Lompounds In the Method Blank of this extraction batch were IND less than the method Rl with the following exceptions <br /> VONT' <br /> BATCH 19884 SUM dARY <br /> Sample ID Date Sampled Date Extracted Date Analyzed Sample 10 Date Sampled Date Extracted Date Analyzed <br /> 0601215-00113 V] 06 1 30 PM 1119/06 l/]9/06 7 54 AM 1 0601215 002B 1/16/06 1 40 PM 1/19106 1/19/06 S 39 AM <br /> •01211-003 B ]!16!06 1 20 PM 1/19106 1119/06 9 23 Aro I __ <br /> MS=Matrix Spike MSD=Matrix Spike Duplicate LCS=Laboratory Control Sample LCSD=LatxaratoryCertrel Sample Duplicate RPD=Relative Percent Deviation <br /> %Recovery=100'(MS-Sample)/(Amount SpLked) RPD=100'(MS- MSD)I((MS+MSD)/2) <br /> MS/MSD spike recoverles and I or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons a)the sample is Inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix Interferes with the spike recovery <br /> NIA=not enough sample to perform matrix spike and matrx spike duplicate <br /> NR=analyle concentration In sample exceeds splke amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content <br /> &2-turyextraction solvents such as methylene chloride and acetone may occasionally ap2ear In the method blank at how levels <br /> DHS Certification No 1644 `P4 QA/QC Officer <br />