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n ! <br /> — I I0 2nd,%�,nne south sl!' Pa<hc(o i A 94551 5560 f <br /> McCampbell Analytical,-Inc. — Ielephom 92] 199 IWO Fix 925 799 1o22 <br /> AVh.lta wwa nX6d11:phellu1ii F 11111 uxuuamKLdniphell..nni <br /> QC SUMMARY REPORT FOR SW8021B/80t5Cml <br /> W O Sample Matrix Water QC Matrix Water WorkOrder 0512244 <br /> EPA Method SW8021BI8015Cm Extraction SW5030B BatchlD 19436 Spiked Sample ID 0512258-005A <br /> Analyte -Sample Spiked _ MS MSD k MS-MSD LCS LCSD LCS-LCSD Acceptance Cntena <br /> pg/L 1tgIL % Rec i % Rec ; %RPD %Rec % Rec %RPD MS/MSD i LCS 1 LCSD <br /> I PI 1(btex)e ND 60 104 102 238 101 102 1 30 70- 130 70- 130 <br /> MTBE ND 10 87 5 88 9 1 59 844 845 0 132 70 130 70 130 <br /> Bcna.nL ND 10 882 889 0 798 846 861 174 70-130 70- 130 <br /> I nluene ND 10 89 5 882 ' 150 845 961 190 70-130 70-130 <br /> Ethylbcntt,nt ND to 913 - 908 0 533 88 3 895- l 42 70-130 70-130 <br /> Xylenes N1) 30 947 943 0353 90 , 907 0 738 70- 130 70-130 <br /> °/nSS 99 10 99 99 1 0 99 98 0 708 70- 130 70-130 <br /> 411 target Lompounds to the Method Blank of this uctraction batch weie ND less than tht,ntLthod KL with the following exceptions <br /> NONE <br /> BATCH 19436 SUMMARY <br /> tairnple ID Date Sampled Date Extracted Date Analyzed Sample ID Date Sampled Date Extracted Date Analyzed <br /> 2244-OOIA 12113'05 12 30 PM 12/15/05 12115'05 8 21 AMU 12244-002A 12/11105 12 45 PM 12/15/05 12/15/05 12 56 AM <br /> 0S 12244-003A 12113/05 12 50 PM 12/15/05 12/15 05 8 51 AM <br /> MS=Matrix Spike MSD=Matrix Spike Duplicate LCS=Laboratory Control Sample LCSD=Laboratory Control Sample Duplicate RPD=Relative Percent Deviation <br /> %Recovery=100'(MS-Sample)I(Amount Spiked),RPD=100'(MS- MSD)/((MS+MSD)12) <br /> MS 1 MSD spike recoveries and/or%RPD may fait outside of laboratory acceptance cntena due to one or more of the following reasons a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked or b)the spiked sample's matrix Interferes with the spike recovery <br /> E TPH(btex)=sum of BTEX areas from the FID <br /> #cluttered chromatogram sample peak cmlutes with surrogate peak <br /> I A=not applicable or not enough sample to perform matrix spike and matnx spike duplicate <br /> NR=analyte concentration In sample exceeds s iko amount for soll matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matnx or analyte content <br /> DHS Certification No 1644 QA/QC Officer <br />