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a U <br /> 4 1102nd A lienor Month If)7 Pathecii ( A 145'i 5,t ) <br /> h <br /> cCalmpbell knalyfical, lot, IPIPPImnP -7aX 162( f 925 79R 1c,2 <br /> - ' _�. � — tt'ehvite wttw okr a,np1.'_«.--��c II<nnt E n><�rl 1rGaiirLulrxc m�l�eil enm -- —1 <br /> . QC SUMMARY REPORT FOR SW8260B <br /> W O Sample Matrix Water QC Matrix Water WcrkOrder 0512244 <br /> EPA Method SW8260B Extraction SW5030B BatchID 19437 Spiked Sample ID 0512240-0018 <br /> Analyte Sample Spiked MS MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria{%) <br /> pg/L pglL % Rec % Rec % RPD %Rec %Rec % RPD MS/MSD LCS/LCSD <br /> teit-Amyl mcthyl i Cher(TAML) ND 10118 119 0 719 103 107 442 70- 130 70- 130 <br /> — <br /> F <br /> It Butyl alcohol(TBA) ND 50 102 106 149 868 898 343 70- 130 70-130 <br /> Dnsupropyl ether(D1PE) ND 10 111 Hi S 3 82 974 ~ 987 1 32 70- 130 70 110 <br /> I thyl tort-butyl ether(ETSE) NO 10 106 110 r 3 30 91 8 944 276 70- 110 70 l 30 <br /> Methyl t-butyl Lthi-r(MTBE) ND 10 106 113 440 927 944 1 183 — 70- 130 70-130 <br /> X51 109 10 101 103 1 81 98 100 222 70- 130 70 130 <br /> All target compounds in the Method Blank of this exti-action batch wt,t-c ND less than the method RL with the following exceptions <br /> NONr <br /> BATCH 19437 SUMMARY <br /> Sample ID Date Sampled Date Extracted Date Analyzed Sample ID� Date Sampled Data Extracted Date Analyzed <br /> 0512244-OOIC 12/13/05 12 30 PM 12/15105 12/1i/05 2 53 AM , 0512244-002B 12113!05 12 45 PM 12/15,05 I2l15105 3 36 AM <br /> 2244--OOIB 1211/105 12 50 PM t2115/05 12/15/00 4 I9 AM — <br /> MS=Matrix Spike,MSD=Matrix Spike Duplicate,LCS=Laboratory Control Sample LCSD=Laboratory Control Sample Duplicate RPD=Relative Percent De%ahon <br /> %Recovery=100*(MS Sample)/(Amount Spiked),RPD=100*(MS MSD)/((MS+MSD)12) <br /> MS I MSD spike recoveries and I or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons a)the sample Is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked orb)the spiked sample's matrix interferes with the splke recovery <br /> NIA=not enough sample to perform matrix spike and matrix spike duplicate <br /> NR=analyte concentration In sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content <br /> Wratory extract on solvents such as methyiene chlonde and acetone may occasfonal;x aRE2ar In the method blank at low levels <br /> DIIS Certification No 1644 U� QA/QC Officer <br />