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Inc )IJ and Avenue 1,nudl tri j I al.hec n i A a-i„3 %6�I <br /> �� cCampbeB Analytical, nI ucphMl(, ')7] 'V1. 1611; 1 o, 01, 9x 1621 <br /> w metal i irtx 11 a nm Email iriimamcevmphell ion -� <br /> QC SUMMARY REPORT FOR S'W8021 B/8015Cm <br /> W O Sample Matrix Water QC Matnx Water Workerder 0511334 <br /> EPAMethod 5W8021B18015Cm Extraction SW5030B BatchlD 19056 Spiked Sample ID 0591334-001A <br /> Analyte Sample Spiked MS MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria{%) <br /> pg/L pg/L. % Rec % Rec % RPD % Rec —% Rec % RPD MS/MSD LCS 1 LCSD <br /> f PW(btux}E ND GO l I S 112 2 57 105 101 3 22 70- 130 70- ]30 <br /> M 13E ND f0 78 7 '9 7 128 861 928 752 70 110 70 130 <br /> Ben7ere ND 10 102 107 444 96 3 997 346 70- 130 70- 130 <br /> Toluene NI) 10 1 1 l 114 282 98 3 107 8 16 70- 130 70- 130 <br /> Fthylbcncane ND 10 114 i 116 1 73 103 105 _ 1 59 70- 1 30 70- 130 <br /> Xvlenes ND 30 t07 107 0 91 3 1 913 0 70 t3o 70 130 <br /> %SS 106 1 10 105 107 164 101 103 203 70-130 70- l 3U <br /> k1I laigt,l Lumpoundv in the Method Blank of thic extraction batch weie ND less than the method Rl with the tollowing LXLeptions <br /> NON L <br /> BATCH 1905§SUMMARY <br /> Sample ID Date Sampled Date Extracted Date Analyzed Sample ID Date Sampled Date Extracted Date Analyzed <br /> � <br /> 11114 001A t(/16105 12 00 Pint I II18r05 1]/18/05 5 25 AM 0511334-002A 11,16 05 12 )U PM 1 Ir18/05 111f8,05 � 55 AM <br /> USI 1114-0034 I l/16,05 12 20 PM t1118,05 11/18/05 11 2] AM 05[1334004A 11/16105 12 30 PM 11 19/05 11r19(15 I1 47 AM <br /> MS=Matrix Spike MSD=Matrix Spike Duplicate LCS=Laboratory Control Sample LCSD=Laboratory Control Sample Duplicate RPD=Relative Percent Deviation <br /> %Recovery=100'(MS-Sample)/(Amount Spiked) RPD=100'(MS- MSC)1((MS+MSD)/2) <br /> MS 1 MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons a)the sample is inhomogenous AND <br /> contams significant concentrations of analyte relative to the amount spiked or b)the spiked sample's matrix interferes with the spike recovery <br /> E TPH(btex)=sum of BTEX areas from the FID <br /> #cluttered chromatogram sample peak coelutes with surrogate peak <br /> 0=not applicable or not enough sample 10 perform matrix spike and matrix spike duplicate <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due tohighmatrix or analyte content <br /> DHS Certification No 1644 p/ <br /> QA/QC Off`icet <br />