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nunutifU <br /> ti, l P.iLheck> ( A 3i;,3 —61- <br /> t� cCampbell Analytical, Inc. Irlcphon< <1)1-794 Ir 10 rn% �M IL,„ <br /> tk rhsur w u n v, , iinphc 1t i oni r 1111,111 ll <br /> a mccvnphell nn <br /> QC SUMMARY REPORT FOR SW8260B <br /> W O Sample Matrix Water QC Matrix Water WorkOrder 0511334 <br /> EPA Method SW026021 Extraction SW50308 SatchlD 19065 Spiked Sample iD 0511338-002-A <br /> Analyte Sample Spiked MS MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> Ng/L pg/L %Rec % RBC % RPD % Rec % Rec % RPD MS I MSD -LCS/LCSD <br /> cert-\myl nieth�i ether (TAME) ND t0 109 108 I 0 942 jos 106 1 68 70-130 70- 130 <br /> t-Butyl alcohol(FBA) 6 50 95 91 9 1 290 99 8 87 9 1 12 70- 130 70- 130 <br /> Ihisnitiopyi ether(RIPE) ND 10 1 U 1 997 1 71 977 ICI 3 37 70-130 �- 70- 130 <br /> Ethyl ten-butyl ether(ETBC) ND 10 975 97 5 0 946 — 952 0560 70- 130 70- 130 <br /> Mc thyl-t butyl Lthi r(MTBE) ND 10 101 100 i 0 500 932 97H 4 82 70 130 70- 130 <br /> 1IiSS 1 108 10 100 100 0 t00 99 l 12 70- 130 70- 130 <br /> All t u get compounds in the.MLLbod Blank of this extiaction hatch were ND less than the method RL witl)the following exceptions <br /> NONE <br /> BATCH 19065 SUMMARY <br /> Sample ID Date Sampled Date Extracted Date Analyzed Sample ID Date Sampled Date Extracted Date Analyzed <br /> 0.51 1 331 OUIC 11116'05 12 00 PM I 1/18/05 11/18/05 7 40 PM 0511334-002B 11/16/04 12 10 PM 11/19/05 1;/19/05 l 49 AM <br /> *1 - -- <br /> 11334 UO-A3 ID 16 05 l2 20 PM 11/19/05 11/19/05 2 39 AM 0511334-004B 1 lr 16/05 12 30 PM 1 1119105 11!19'05 3.27 AM <br /> MS=Matrix Spike MSD=Matrix Spike Duplicate LCS=Laboratory Control Sample LCSD=Laboratory Control Sample Duplicate,RPD=Relative Percent Deviation <br /> %Recovery=100'(MS-Sample)/(Amount Spiked) RPD=100.(MS- MSD)/((MS+MSD)/2) <br /> MS 1 MSD spike recoveries and 1 or%RPD may fall outside of laboratory acceptance criteria due to one or more of the fallowing reasons a)the sample is mhomcgenous AND <br /> contains signlficarit concentrations of analyte relative to the amount spiked or b)the spiked sample's matrix Interferes with the spike recovery <br /> NIA=not enough sample to perform matrix spike and matrix spike duplicate <br /> NR=analyte concentration in sample exceeds spike amount for soil malnx or exceeds 2x spike amount for water matrix or sampie diluted due to high matrix or analyte content <br /> Ibcralkory extraction solvents such as meth ene chloride and acetone may occasionally appear In the method blank at low levels <br /> DHS Certification No 1644 QA/QC Officex <br />