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i <br /> 110 2nd Avenue South i107 Pachcco CA 94553 5560 <br /> t tical, Inc. =elephn,re 925 s m 98 Fax 925 71622 nvb <br /> Wehsric www rtrtcar�hellell cam E marl rnevt r�i mccan�bel <br /> McCampbell Analytical, enrat <br />�y ...4.i.-._ . �� _ - �„ ..... .+.n _ .. ...-y--rte-�•w- " w -y��..3��--�i`'��.� '--,•...�..T... ............. wY'<w1-.-..sve'...• <br /> TQC SUMMARY REPORT FOR SW8260B _ '� <br /> 1 WarkOrder 0505425 <br /> W O Sample Matrix Water QC Matrix Water <br />' EPA Method SW8260B Extraction SW30308 BatchiD 16399 Spiked Sample ID 050542"010 <br /> Sample Spiked MS MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(°k) <br /> Analyte <br /> uglL liglL % Rec %Rec %RPD %Rec %Rec %RPD MS I MSD ILCSILCSD <br /> tent-Amyl methyl ether(rAMI;) ND L O 117 1 l6 0903 111 Its 609 _ 70-130 70- 130 <br /> t-Butyl alcohol(TBA) ND 50 913 905 D 860 929 969 422 70 130 70-130 <br />' Dusopropyl ether(DIPS) - ND 10 119 119 0 119 119 0 7,0-130 70-130 <br /> Ethyl tert-butyV ether(ETBC) ND l0 114 113 _0 998 110 114 3 SS 70- 134 <br /> Methyl t-butyl ether(MTBE) 0 99 10 110 109 0 517 108 114 70-130 70- 130 <br /> 5 45 <br /> %SS1 96 l0 10! 98 298 99- 98 130 70-130 70-130 <br /> All target compounds to the Method Blank of this extraction batch were ND tesa than the method RL with the following exceptions <br /> NONE <br /> BATCH 16399 SQMMARY <br /> Sample ID Date Sampled Date Extracted Date Analyzed Sample ID Date Sampled _Date Extracted Date Analyzed <br />' 0505425-OO1C 5126!05 2 00 PM 5127105 5127105 6 54 PM —— <br /> 1 MS=Matrix Spike,MSD=Matrix Splke Duplicate,LCS=Laboratory Contml Sample LCSD=Laboratory Control Sample Duplicate RPD=ReleWe Percent Deviation <br /> %Recovery=10D•(MS Sample)I(Amount Spiked) RPD=t00•(MS- MSD)I((MS+MSD)12) <br /> ' MS 1 MSD spike recoveries and I or%RPD may fall outside of laboratory acceptance cdtshe due to one or more of the Following reasons a)the sample is Inhomogenous AND <br /> contains signrd concentfa6ans of analyte relative to the amount spiked or b)the spiked sample s matnx interferes with the spike recovery <br /> �ra <br /> NrA=not enough sample to perforin matrix spike and matrix spike duplicate <br /> ' NR=analyte concentration in sample exceeds Spike amount for sod matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content <br /> Laboratoa extraction solvents such es mesh ne chloride and acetone may accasiorally appear in the method blank at low levels <br /> [ <br /> ' DHS Certification No 1644 1-QA/QC Officer <br /> 1 <br />