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I <br /> 110 21nd Aveuae South,tlD7 Pacheco CA 94553 5560 <br /> 1N4- �McCam bell Analytical, Inc., Teletrhane 925 798-1620 Fax 925-798 1622 �w..w <br /> P "Websutl wwwmccsrripbellcom 13 ma0 m3mr�iriecaiophel!eem.-.�-�_ =:•"���=`��=�=V'�= <br /> M ~~ r TQC SUMMARY REPORT FOR SW8021B/8015Cm�� <br /> W O Sample Matrix Air QC Matrix Water WorkOrder 0505424 <br />' EPA Method SW80218I801SCrn Elctrechon SW5030B BatehlD 16388 Spiked Sample lD 0505425-004A <br /> Sample Spiked MS MSD MS-MSD' LCS LCSD !LCS-LCSD Acceptance Criteria(°k) <br /> Analyte -- — — — — -- <br /> ltglL NglL %Rae I °A Rec %RPD %Reo -4 Ree %RPD MS!MSD LCS 1 LCSD <br />' ]PH(btex)£ NO 60 930 951 j 1 65 94 906 280 70- 130 70- 130 <br /> MTB -- ND to - 887 ! 821 778 805 I 957 628 70-130 70- 130 <br />' Benzene _ ND 10 102 I 97 7 3 87 993 103 405 70 136 1 _70- 130 <br /> — �- <br /> Tolucne ND 10 104 E 101 _L 2 I S 104 I l0$ 4]8 7D-Y130 70-130 <br />' Ethvlbenzene _ ND to 105 103_ I 142 104 107 ! 263 74 130 741- 130 ry <br /> X-lenes ND 30 91 9[ 0 �91 9-53 , 4 65 70-110 70 134 <br /> °i°SS 1 1 t 10 114 112 2 36 110 112 172 70- 110 70- 134 <br /> All target compounds in the Method Blank n1 this extmetion batch were ND less than the method RL with the tollowmg exceptions <br /> NONF <br /> BATCH 18388 SUMMARY <br />' Sample ID Date Sampled Date Extracted —Date Analyzed Sample ID— Date Sampled Date Extracted Date Analyzed <br /> 0505424-001 A 5126105 1 45 PM 5127/05 5127105 5 50 PM <br /> I <br /> 1 <br /> 1 <br /> i <br /> M5=Matrix Spike MSD=Matrix Spike Duplicate LCS=Laboratory Control Sample LCSD=Laboratory Control Sample Duplicate RPD=Relative Percent Deviation <br /> Recovery=loo•(NAS Sample)!(Amount Spiked),RPD=100`(MS- MSD)1((MS+MSD)12) <br /> MS!MSD spike recoveries and 1 or%RPD may fall outside of laboratory acceptance criteria due to one or more of the Following reasons a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked or b)the spiked sample s matrix interferes wrath the spike recovery <br /> £TPH(btex)=sum of BTEX areas from the FID <br /> #Guttered chromatogram sample peak coelutes with surrogate peak <br /> NIA=not enough sample to perform matrix spke and matrix spike duplicate <br /> NR=anatyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matnx or sample diluted due to high matrix or analyte content <br /> DHS Certification No 1644 J X A QC Officer <br /> 1 <br />