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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> h //www mccam bell com E-mail main@mccampbell com <br /> Ground Zero Analysis, Inc Client Project ID #256,Gabbard Date Sampled 10/25-10/27/99 <br /> 1714 Main Street Date Received 10/29/99 <br /> Escalon,CA 95320 Client Contact John Lane Date Extracted 10/29/99 <br /> Client P O Date Analyzed 11/02-11/08/99 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab 1D 24361 <br /> Client ID GAB S85GW-26 <br /> Matnx W <br /> Compound Concentration* Compound Concentration* <br /> Acetone i ND<6 trans-l,3-Dichloropropene ND <br /> Benzene 6 9 Ethylene dibromide ND <br /> Bromobenzene ND Ethylbenzene 13 <br /> Bromochloromethane ND Hexachlorobutadiene ND <br /> Bromodichloromethane ND lodomethane ND <br /> Bromoform ND Isopropylbenzene 33 <br /> Bromomethane ND p-Isopropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketone ND <br /> sec-Butyl benzene ND Methylene Chlonde` ND<2 <br /> tert-Butyl benzene ND Methyl ethyl ketone ND <br /> Carbon Disulfide ND Methyl isobutyl ketone 101 ND <br /> Carbon Tetrachloride ND Methyl tert-Butyl Ether(MTBE) <br />• Chlorobenzene l6 Naphthalene ND <br /> Chloroethane ND n-Propyl benzene 3 9 <br /> 2-Chloroethyl Vinyl Ether"' ND Styrene ND <br /> Chloroform ND 1,1,1,2-Tetrachloroethane ND <br /> Chloromethane ND 1,1,2,2-Tetrachloroethane ND <br /> 2-Chlorotoluene ND Tetrachloroethene ND<20 <br /> 4-Chlorotoluene ND Toluene"1 14 <br /> Dibromochloromethane ND 1,2,3-Tnchlorobenzene ND <br /> 1,2-Dibromo-3-chloropropane ND 1,2,4-Tnchlorobenzene ND <br /> Dibromomethane ND 1,1,1-Trichloroethane ND <br /> 1,2-Dichlorobenzene 23 1,1,2-Tnchloroethane N D <br /> l,3-Dichlorobenzene 2 7 Trichloroethene ND <br /> 1,4-Dichlorobenzene 2 7 Trichlorofluoromethane ND <br /> Dichlorodifluoromethane ND 1,2,3-Tnchloropropane ND <br /> l,l-Dichloroethane ND 1,2,4-Tnmethylbenzene 15 <br /> 1,2-Dichloroethane ND 1,3,5-Tnmethylbenzene 25 <br /> 71-Dichloroethene ND Vinyl Acetate ° ND <br /> cis-1,2-Dichloroethene 32 Vinyl Chlonde ° ND <br /> trans-1,2-Dichloroethene ND Xylenes,total 22 <br /> 1,2-Dichloropropane ND Comments <br /> 1,3-Dtchloropropane ND Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND Dibromofluoromethane 100 <br /> 71-Dichlorop open ND Toluene-d8 106 <br /> cis-1,3-Dichloropropene ND 4-Bromofluorobenzene 88 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I SDLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 uglL,vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2 <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment, U) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />