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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//wwwmccampbellco E-mail main@mccampbell com <br /> Ground Zero Analysis,Inc CIient Project ID #256,Gabbard Date Sampled 10/25-10/27199 <br /> 1714 Main Street Date Received 10/29/99 <br /> Escalon,CA 95320 Client Contact John Lane Date Extracted 10/29/99 <br /> Client P O Date Analyzed 11/02-11/0899 <br /> Volatile Organics By GC/M5 <br /> EPA method 8260 <br /> Lab ID 24364 <br /> Client ID GAB SB6-20 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<450 trans-1,3-Dtchloropropene ND<130 <br /> Benzene ND<130 Ethylene dibromide ND<130 <br /> Bromobenzene ND<130 Ethylbenzene 300 <br /> Bromochloromethane ND<130 Hexachlorobutadiene ND<130 <br /> Bromodichloromethane ND<130 Iodomethane ND<130 <br /> Bromoform ND<130 Isopropylbenzene 1300 <br /> Bromomethane ND<130 p-Isopropyl toluene ND<130 <br /> n-Butyl benzene 1400 Methyl butyl ketone ND<130 <br /> sec-Butyl benzene 1000 Methylene Chlonde° ND<130 <br /> tert-Butyl benzene ND<130 Methyl ethyl ketone ND<130 <br /> Carbon Disulfide ND<130 Methyl isobutyl ketone'8' ND<130 <br /> Carbon Tetrachloride ND<130 Methyl tert-Butyl Ether(MTBE) — <br />• Chlorobenzene ND<130 Naphthalene ND<130 <br /> Chloroethane ND<130 n-Propyl benzene 2000 <br /> 2-Chloroethyl Vinyl Ether() ND<130 Styrene ND<130 <br /> Chloroform ND<130 1,1,1,2-Tetrachloroethane ND<130 <br /> Chloromethane ND<130 1,1,2,2-Tetrachloroethane ND<130 <br /> 2-Chlorotoluene 270 Tetrachloroethene ND<130 <br /> 4-Chlorotoluene ND<130 Toluene"' 890 <br /> Dibromochloromethane ND<130 1,2,3-Tnchlorobenzene ND<130 <br /> 1,2-Dibromo-3-chioropropane ND<130 1,2,4-Tnchlorobenzene ND<130 <br /> Dibromomethane ND<130 1,1,1-Tnchloroethane ND<t 30 <br /> 1,2-Dichlorobenzene ND<130 1,1,2-Tnchloroethane ND<130 <br /> 1,3-Dtchlorobenzene ND<130 Trichloroethene ND<130 <br /> 1,4-Dichlorobenzene ND<130 Trichlorofluoromethane ND<130 <br /> Dichlorodifluoromethane ND<130 1,2,3-Tnchloropropane ND<130 <br /> l,l-Dichloroethane ND<130 1,2,4-Tnmethylbenzene 650 <br /> 1,2-Dichloroethane ND<130 1,3,5-Tnmethylbenzene 250 <br /> 1,1-Dichloroethene ND<130 Vinyl Acetate ND<130 <br /> cis-1,2-Dichloroethene ND<130 Vinyl Chloride(0) ND<130 <br /> trans-1,2-Dichloroethene ND<130 Xylenes,total IPI 2100 <br /> 1,2-Dichloropropane ND<130 Comments <br /> 1,3-Dichloropropane ND<130 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND<130 Dibromofluoromethane 99 <br /> 71-Dtchloropropene ND<130 Toluene-d8 130 <br /> cis-t,3-Dtchloropropene ND<130 4-Bromofluorobenzene 114 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples I ug/L,vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2 <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than—5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (I) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />