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4 <br /> 110 2nd Avenue South,##D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//w-wwmccampbellco E-mail main@mccampbell com <br /> • <br /> Ground Zero Analysts,Inc Client Project ID #256, Gabbard Date Sampled 10/25-10/27/99 <br /> 1714 Main Street Date Received 10/29/99 <br /> Escalon,CA 95320 Client Contact John Lane Date Extracted 10/29/99 <br /> Client P O Date Analyzed 11/02-11/08/99 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 24377 <br /> Client ID GAB SB8GW-26 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone N1<6 trans-l,3-Dichloropropene ND <br /> Benzene ND Ethylene dibromide ND <br /> Bromobenzene ND Ethylbenzene ND <br /> Bromochloromethane ND Hexachlorobutadiene ND <br /> Bromodichloromethane ND lodomethane ND <br /> Bromoform ND Isopropylbenzene ND <br /> Bromomethane ND p-Isopropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketone ND <br /> sec-Butyl benzene ND Methylene Chlonde"J N1X2 <br /> tert-Butyl benzene ND Methyl ethyl ketone ND <br /> Carbon Disulfide ND Methyl isobutyl ketoneTsT ND <br /> Carbon Tetrachloride ND Methyl tent-Butyl Ether(MTBE) <br /> Chlorobenzene ND Naphthalene ND <br /> Chloroethane ND n-Propyl benzene ND <br /> 2-Chloroethyl Vinyl Ether"' ND Styrene ND <br /> Chloroform ND 1,1,1,2-Tetrachloroethane ND <br /> Chloromethane ND 1,1,2,2-Tetrachloroethane ND <br /> 2-Chlorotoluene ND Tetrachloroethene ND¢20 <br /> 4-Chlorotoluene ND Toluene m ND <br /> Dtbromoehloromethane ND 1,2,3-Tnchlorobenzene ND <br /> 1,2-Dibromo-3-chloropropane ND 1,2,4-Tnchlorobenzene ND <br /> Dibromomethane ND 1,1,1-Tnchloroethane ND <br /> 1,2-Dichlorobenzene ND 1,1,2-Tnchloroethane ND <br /> 1,3-Dichlorobenzene ND Tnchloroethene ND <br /> 1,4-Dichlorobenzene ND Trichlorofluoromethane ND <br /> Dichlorodifluoromethane ND 1,2,3-Tnchl0ropr0pane ND <br /> 1,1-Dichloroethane ND 1,2,4-Tnmethylbenzene ND <br /> 1,2-Dichloroethane ND 1,3,5-Tnmethylbenzene ND <br /> 1,1-Dichloroethene ND Vinyl Acetate " ND <br /> cis-1,2-Dichloroethene ND Vinyl Chloride ° ND <br /> trans-1,2-Dichloroethene ND Xylenes,total ND <br /> 1,2-Dichloropropane ND Comments <br /> 1,3-Dichloropropane ND Surrogate Recoveries <br /> 2,2-Dichloropropane ND Dibromofluoromethane 99 <br /> 771-Dtchloropropene ND Toluene-d8 107 <br /> cis-1,3-Dtchloropropene ND 4-Bromofluorobenzene 88 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 ug/L,vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysts <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2 <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than—5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edvrard Hamilton,Lab Director <br />