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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCA TBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccanipbell coni E-mail main@mccampbell com <br /> Ground Zero Analysis,Inc Client Protect ID #256,Gabbard Date Sampled 10/25-10/27/99 <br /> 1714 Main Street Date Received 10/29/99 <br /> Escalon, CA 95320 Client Contact John Lane Date Extracted 10/29/99 <br /> Client P O Date Analyzed 10/29-11/01/99 <br /> Lead* <br /> EPA analytical methods 6010/200 7,239 2+ <br /> Lab ID Client ID Matrix Extraction° Lead* %Recovery <br /> Surrogate <br /> 24376 GAB SB8-31 S TTLC 68 99 <br /> 24377 GAB SBGW-26 W TTLC 033 NA <br /> 24378 GAB SB6-25 S TTLC 47 102 <br />• <br /> S TTLC 3 0 mg/kg <br /> Reporting Limit unless otherwise <br /> stated,ND means not detected above W TTLC 0 005 mg/L <br /> the reporting linut <br /> --- STLC,TCLP 0 2 mg/L <br /> *soil and sludge samples are reported in mg/kg,wipe samples in ug/wipe,and water samples and all STLC I SPLP I TCLP extracts in mg/L <br /> `Lead is analysed using EPA method 6010 (ICP)for soils, sludges, STLC & TCLP extracts and method 239 2 (AA Furnace) for water <br /> samples <br /> °EPA extraction methods 1311(TCLP),3010/3020(water,TTLC),3040(organic matrices,TTLC),3050(solids,TTLC),STLC-CA Title 22 <br /> "surrogate diluted out of range,N/A means surrogate not applicable to this analysis <br /> reporting lirrut raised due matrix interference <br /> • i) liquid sample that contains greater than --2 vol % sediment, this sediment is extracted with the liquid, in accordance with EPA <br /> methodologies and can significantly effect reported metal concentrations r <br /> DHS Certification No 1644 s 1r Edward Hamilton, Lab Director <br />