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110 2nd Ave South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> UM//www mccampbelI com E-mail main@mccampbell com <br /> Ground Zero Analysts,Inc Client Project ID #256,Gabbard Date Sampledtoj/9 <br /> 1714 Main Street Date Received 01/21/99 <br /> Escalon,CA 95320 Client Contact John Lane Date Extracted 01/22-01/25199 <br /> Client P O Date Analyzed 01123-01/28/99 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 02119 <br /> Client ID GASB 1-21 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<2000 Ethylbcnzene ND<2000 <br /> Benzene ND<2000 Hexachlorobutadiene ND<2000 <br /> Bromobenzene ND<2000 lodomethane ND<2000 <br /> Bromochloromethane ND<2000 Isopropylbenzene 4000 <br /> Bromodichloromethane ND<2000 p-Isopropyl toluene ND<2000 <br /> Bromoform ND<2000 Methyl butyl ketone ND<2000 <br /> Bromomethane ND<2000 Methylene Chloride` ND<2000 <br /> n-Butyl benzene 7100 Methyl ethyl ketone ND<2000 <br /> sec-Butyl benzene 6600 Methyl isobutyl ketone ND<2000 <br /> tert-Butyl benzene ND<2000 Methyl tert-Butyl Ether(MTBE) _- <br /> Carbon Disulfide ND<2000 Naphthalene 8100 <br /> • Carbon Tetrachlonde ND<2000 n-Propyl benzene 8400 <br /> Chlorobenzene ND<2000 Styrene ND<2000 <br /> Chloroethane ND<2000 1,1,1,2-Tetrachloroethane ND<2000 <br /> 2-Chloroethyl Vinyl—Ethe—r`T ND<2000 M 22-Tetrachloroethane ND<2000 <br /> Chloroform ND<2000 Tetrachloroethene ND<2000 <br /> Chloromethane ND<2000 Toluene MND<2000 <br /> 2-Chlorotoluene ND<2000 1,2,3-Tnchlorobenzene ND<2000 <br /> 4-Chlorotoluene ND<2000 1,2,4-TTchlorobenzene ND<2000 <br /> Dibromochloromethane ND<2000 1,1,1-Trichloroethane ND<2000 <br /> 1,2-Dibromo-3-chloropropanc ND<2000 1,1,2-Tnchloroethane ND<2000 <br /> Dibromomethane ND<2000 Tnchloroethene ND<2000 <br /> 1,2-Dichlorobenzene ND<2000 Trichlorofluoromethane ND<2000 <br /> 1,3-Dichlorobenzene ND<2000 1,2,3-Tnchloropropane ND<2000 <br /> 1,4-Dichlorobenzene ND<2000 1,2,4-Tnmethylbenzene ND<2000 <br /> Dichlorodifluoromethane ND<2000 1,3,5-Tnmethylbenzene ND<2000 <br /> 1,I-Dichloroethane ND<2000 Vinyl Acetate m ND<2000 <br /> 1,2-Dichloroethane ND<2000 Vinyl Chloride ° NIK2000 <br /> l,l-Dichloroethene ND<2000 Xylenes,total ND<2000 <br /> cis-1,2-Di chloroethene ND<2000 TPH-(g)(C6-C12) <br /> trans-1,2-Dichloroethene ND<2000 TPH-(ms)(C8-C 12) -- <br /> 1,2-Dichloropropane ND<2000 TPH-(k)(C 10+) -- <br /> 1,3-Dichloropropane ND<2000 <br /> 2,2-Dichloropropane ND<2000 Comments <br /> ],I-Dichloropropene ND<2000 Surrogate Recoveries(%) <br /> cis-1,3-Dichloropropene ND<2000 Dibromofluoromethane 100 <br /> trans-1,3-Dichlompropene ND<2000 Toluene-d8 92 <br /> Ethylene dibromide ND<2000 4-Bromofluorobenzene 109 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 10 ug/L, vapor samples 0 5 ug/L, solid and sludge samples 5 0 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d)2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i) liquid sample that contains greater than —5 vol <br /> sediment,(l)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,0)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />