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1 � <br /> tJ <br /> 110 2nd Ave South,##D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> bttp llwww mccampbell com E-mail main@mccampbell com <br /> • <br /> Ground Zero Analysts, IncDate Sampled 01/20/99 <br /> Client Project ID #256,Gabbard <br /> 1714 Main Street Date Received 01/21/99 <br /> Escalon, CA 95320 Client Contact John Lane Date Extracted 01/22/99 <br /> Client P O Date Analyzed 01/23-01/24/99 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 02123 <br /> Client ID GASB2-21 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br /> Acetone" ND Ethylbenzene ND <br /> Benzene ND Hexachlorobutadiene ND <br /> Bromobenzene ND lodomethane ND <br /> Bromochloromethane s ND Isopropylbenzene ND <br /> Bromodichloromethane ND p-Isopropyl toluene ND <br /> Bromoform ND Methyl butyl ketone ND <br /> Bromomethane ND Methylene Chlonde° ND<15 <br /> n-Butyl benzene ND Methyl ethyl ketone ND <br /> sec-Butyl benzene ND Methyl isobutyl ketone is ND <br /> tert-Butyl benzene ND Methyl tert-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND Naphthalene ND <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> Chlorobenzene ND Styrene ND <br /> Chloroethane ND 1,1,1,2-Tetrachloroethane ND <br /> 2-Chloroethyl Vinyl Ether" ND 1,1,2,2-Tetrachloroethane ND <br /> Chloroform ND Tetrachloroethene ND<15 <br /> Chloromethane ND Toluene ND <br /> 2-Chlorotoluene ND 1,2,3-Trichlorobenzene ND <br /> 4-Chlorotoluene ND 1,2,4-Tnchlorobenzene ND <br /> Dibromochloromethane ND 1,1,1-Tnchloroethane ND <br /> 1,2-Dibromo-3-chloropropane ND 1,1,2-Trichloroethane ND <br /> Dibromomethane ND Trichloroethene ND <br /> 1,2-Dichlorobenzene ND Tnchlorofluoromethane ND <br /> 1,3-Dichlorobenzene ND 1,2,3-Tnchloropropane ND <br /> 1,4-Dichlorobenzene ND 1,2,4-Tnmethylbenzene ND <br /> Dichlorodifluoromethane ND 1,3,5-Tnmethylbenzene ND <br /> l,]-Dichloroethane ND Vinyl Acetate ND <br /> 1,2-Dichloroethane ND Vinyl Chlonde " ND <br /> 1,1-Dichloroethene ND Xylenes,total ND <br /> cis-1,2-Dichloroethene ND TPH-(g)(C6-C12) -- <br /> trans-1,2-Dichloroethene ND TPH-(ms)(C8-C12) --- <br /> 1,2-Dichloropropane ND TPH-(k)(C10+) --- <br /> 1,3-Dichloropropane ND <br /> 2,2-Dichloropropane ND Comments <br /> 1,1-Dichloropropene ND Surrogate Recoveries(%) <br /> cis-1,3-Dichloropropene ND Dibromofluoromethane 97 <br /> trans-l,3-Dichloropropene ND Toluene-d8 95 <br /> Ethylene dibromide ND 4-Bromofluorobenzene 94 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L, vapor samples 0 5 ug/L, solid and sludge samples 5 0 ug/kg, wipes <br /> 0 2uglwipe ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,(1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />