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110 2nd Ave South,##D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 12p.1/www mcca=bell com E-mail main@mccampbell com <br /> • <br /> /2 <br /> Ground Zero Analysis,Inc Client Project ID #256,Gabbard Date Sampled 0 0/99 <br /> 1714 Main Street Date Received 01 9 <br /> Escalon,CA 95320 Client Contact John Lane Date Extracted 01/22-01/25/99 <br /> Client P O Date Analyzed 01/23-01/28/99 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 02125 <br /> Client ID GASB3-6, <br /> Matrix S, <br /> Compound Concentration* Compound Concentration* <br /> Acetone 720 Ethylbenzene 600 <br /> Benzene ND<150 Hexachlorobutadtene ND<150 <br /> Bromobenzene ND<150 lodomethane ND<150 <br /> Bromochloromethane N13<150 Isopropylbenzene ND<150 <br /> Bromodichloromethane ND<150 p-Isopropyl toluene ND<150 <br /> Bromoform ND<150 Methyl butyl ketone ND<150 <br /> Bromomethane ND<150 Methylene Chlonde` N13<150 <br /> n-Butyl benzene 440 Methyl ethyl ketone ND<150 <br /> sec-Butyl benzene 150 Methyl isobutyl ketone i8 910 <br /> tert-Butyl benzene ND<150 Methyl tert-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND<150 Naphthalene 1500 <br /> Carbon Tetrachloride ND<150 n-Propyl benzene 620 <br /> Chlorobenzene ND<150 Styrene ND<150 <br /> Chloroethane ND<150 1,1,1,2-Tetrachloroethane ND<150 <br /> 2-Chloroethyl Vinyl Ethe ND<150 1,1,2,2-Tetrachloroethane ND<150 <br /> Chloroform ND<150 Tetrachloroethene ND<430 <br /> Chloromethane ND<150 Toluene 1100 <br /> 2-Chlorotoluene N D<l 50 1,2,3-Tnchlorobenzene ND<150 <br /> 4-Chlorotoluene ND<150 1,2,4-Tnchlorobenzene ND<150 <br /> Dibromochloromethane ND<150 1,1,1-Tnchloroethane ND<150 <br /> 1,2-Dibromo-3-chloropropane ND<150 1,1,2-Tnchloroethane ND<150 <br /> Dibromomethane ND<150 Tnchloroethene ND<150 <br /> 1,2-Dichlorobenzene ND<150 Tnchlorofluoromethane ND<150 <br /> 1,3-Dichlorobenzene ND<150 1,2,3-Tnchloropropane ND<150 <br /> 1,4-Dichlorobenzene ND<150 l,2,4-Tnmethylbenzene 4800 <br /> Dichlorodifluoromethane ND<150 1,3,5-Tnmethylbenzene 1800 <br /> I,1-Dichloroethanc ND<150 Vinyl Acetate"' ND<150 <br /> 1,2-Dichloroethane ND<150 Vinyl Chloride " ND<150 <br /> 1,1-Dichloroethene ND<150 Xylenes,total 4100 <br /> cis-1,2-Dtchloroethene ND<150 TPH-(g)(C6-C12) --- <br /> trans-1,2-Dtchloroethene ND<150 TPH-(ms)(C8-C12) -- <br /> 12-Dtchloropropane ND<150 TPH-(k)(C10+) --- <br /> 1,3-Dtchloropropane ND<150 <br /> 2,2-Dtchloropropane ND<150 Comments <br /> IJ-Dtchloropropene ND<150 Surrogate Recoveries <br /> cis-1,3-Dtchloropropene ND<150 Dibromofluoromethane 98 <br /> trans-l,3-Dtchloropropene ND<150 Toluene-d8 98 <br /> Ethylene dibromide ND<150 4-Bromofluorobenzene 123 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes to ug/wtpe and all TCLP/SPLP extracts to ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L, vapor samples 0 5 ug/L, solid and sludge samples 5 0 ug/kg wipes <br /> 0 2u&/wipe ND means not detected above the reporting hmtt,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i) liquid sample that contains greater than —5 vol % <br /> sediment,0)sample diluted due to high organic content, (k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte (1)methylbenzene (m)acetic acid ethenyl ester,(n)chloroethene,(o)dimetbylbenzenes <br /> DHS Certification No 1644 // Edward Hamilton,Lab Director <br />