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110 2nd Ave South,4D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> hhIM//www mccampbell gg E-mail main@mccampbcll corn <br /> Ground Zero Analysts,Inc Client Project ID 4256,Gabbard Date Sampled 0 /20/99 <br /> 1714 Main Street Date Received 01/21/99 <br /> Escalon,CA 95320 Client Contact John Lane Date Extracted 01122-01125199 <br /> Client P O Date Analyzed 01/23-01128199 <br /> Volatile Organics By GUMS <br /> EPA method 8260 <br /> Lab 1D 02127 <br /> Client ID GAS133-31 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<670 Ethylbenzene ND<670 <br /> Benzene ND<670 Hexachlorobutadiene ND<670 <br /> Bromobenzene ND<670 lodomethane ND<670 <br /> Bromochloromethane ND<670 Isopropylbenzene 910 <br /> Bromodichloromethane ND<670 p-Isopropyl toluene 1800 <br /> B70mOfOrM NIK670 Methyl butyl ketone ND<670 <br /> Bromomethane ND<670 Methylene Chlonde` ND<670 <br /> n-Butyl benzene 2400 Methyl ethyl ketone ND<670 <br /> sec-Butyl benzene 1600 Methyl isobutyl ketones ND<670 <br /> ten-Butyl benzene ND<670 Methyl Cert-Butyl Ether(MTBE) --- <br /> Carbon Dlsulfde ND<670 Naphthalene 7100 <br /> Carbon Tetrachloride ND<670 n-Propyl benzene 910 <br /> Chlorobenzene ND<670 Styrene ND<670 <br /> Chloroethane ND<670 1,1,1,2-Tetrachloroethane ND<670 <br /> 2-Chloroethyl Vinyl Ether` ND<670 1,1,2,2-Tetrachloroethane ND<670 <br /> Chloroform ND<670 Tetrachloroethene ND<670 <br /> Chloromethane ND<670 Toluene ND<670 <br /> 2-Chlorotoluene ND<670 1,2,3-Tnchlorobenzene ND<670 <br /> 4-Chlorotoluene ND<670 1,2,4-Tnchlorobenzene ND<670 <br /> Dibromochloromethane ND<670 1,1,1-Tnchloroethane ND<670 <br /> 1,2-Dibromo-3-chloropropane ND<670 1,1,2-Tnchloroethane ND<670 <br /> Dibromomethane ND<670 Trichloroethene ND<670 <br /> 1,2-Dichlorobenzene 3500 Tnchlorofluoromethane ND<670 <br /> 1,3-Dichlorobenzene ND<670 1,2,3-Trichloropropane ND<670 <br /> 1,4-Dichlorobenzene ND<670 1,2,4-Trimethylbenzene 9900 <br /> Dichlorodifluoromethane ND<670 1,3,5-Tnmethylbenzene 5600 <br /> 1,1-1)ichloroethane ND<670 Vinyl Acetate" ND<670 <br /> 1,2-Dichloroethane ND<670 Vinyl Chloride ° ND<670 <br /> l,l-Dichloroethene ND<670 Xylenes,total ND<670 <br /> cis-1,2-Dichloroethene ND<670 TPH-(g)(C6-C12) --- <br /> trans-1,2-Dichloroethene ND<670 TPH-(ms)(C8-C12) --- <br /> 1,2-Dichloropropane ND<670 TPH-(k)(C10+) <br /> 1,3-Dichloropropane ND<670 <br /> 2,2-Dichloropropane ND<670 Comments <br /> 1,1-Dichloropropene ND<670 Surrogate Recoveries(%) <br /> cis-1,3-Dichloropropene ND<670 Dibromofluoromethane 98 <br /> trans-1,3-Dichloropropene ND<670 Toluene-d8 92 <br /> Ethylene dibmmide ND1670 4-Bromofluorobenzene 103 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L, vapor samples 0 5 ug/L, solid and sludge samples 5 0 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2 butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than--5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,(1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 f// Edward Hamilton,Lab Director <br />