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a <br /> i <br /> - s <br /> 2` FF <br /> A <br /> M <br /> K. Ice the sample vials immediately and keep them iced <br /> through shipment. <br /> L. Fill out chain-of-custody form. SOP 11 gives major <br /> details. Make sure sample requests is for proper <br /> analysis type. <br /> M. . Shipping of hazardous materials (methanol) requires <br /> special documents from Federal Express and UPS. <br /> Briefly you will need to add following to outside of <br /> package and on documents: <br /> 1. Flammable liquid label (some will come from lab <br /> with the vials) . <br /> 2. "UN1230 methyl alcohol". <br /> 3. For UPS, a "Hazardous Material" label. <br /> w N. Ship overnight delivery to the lab. If dry ice is <br /> available, up to 5 pounds per package can be sent via <br /> w. Federal Express by simply writing "ORM-A dry ice, <br /> pounds, for research" on outside of package and on <br /> shipping document. UPS does not accept dry-ice <br /> shipments. <br /> 5. Good sampling practice would include preparing one out of <br /> ;y five samples to be prepared in duplicates for analysis. <br /> These four out of twenty samples will be for the following <br /> purposes: <br /> A. One in every twenty samples should be analyzed as a <br /> field replicate to evaluate the precision of the <br /> sampling technique. A minimum of one sample per <br /> data set is suggested. <br /> B. An additional one in twenty samples should be selected <br /> by sampler to be prepared in duplicate as alternative <br /> - to Step (A) . Choose a different soil type if <br /> available. <br /> C. The lab does spiking with reference materials for <br /> internal Quality Control (QC) so additionally a minimum <br /> of two in twenty samples need to be prepared in <br /> duplicate. <br /> -.- �a CiHOl:�U41'lrkl{ <br /> ... n. TF(:11No1AK,1'Inc. <br />