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819 Striker Avenue'Sulte 8 ' Sequoia Sacramento, 95834 (9 i 6)92 921-9600 FAX Analytical www squo pp labs r equolaabs coin IT Corporation-Sacramento Project Tosco 4409,Stockton,CA 1326 N Market Blvd Protect Number N/A Reported Sacramento CA,95834 Project Manager Kathleen Waldo 09/19/01 16 52 Total Purgeable Hydrocarbons and BTEX by DHS LUFT Sequoia Analytical- Sacramento Reporting Analyte Result Limit Units Dilution Batch Prepared Analyzed Method Notes MW-8@30' (5109022-05)Sod Sampled 08/30/0100 00 Received 09/04/01 17 04 Purgeable Hydrocarbons ND 50 mg/kg 1 1090079 09/07/01 09/07/01 DHS LUFT Benzene ND 0 025 " Toluene ND 0 025 " Ethylbenzene ND 0 025 Xylenes(total) ND 0 025 " Surrogate a,a,a-Trifluorotoluene 105% 60-140 " MW-8@60'(S109022-11)Soil Sampled 08/30/0100 00 Received 09/04/01 17 04 Purgeable Hydrocarbons 50 25 mg/kg 5 1090079 09/07/01 09/07/01 DHS LUFT Benzene 022 0 12 " Toluene 014 012 Ethylbenzene 026 0 12 " Xylenes(total) 035 0 12 " AF-B Surrogate a,a,a-Trifluorotoluene 127% 60-140 " MW-8@80'(S109022-15)Soil Sampled 08/30/0100 00 Received 09/04/01 17 04 . Purgeable Hydrocarbons ND 5 0 mg/kg 1 1090079 09/07/01 09/07/01 DHS LUFT A-01 Benzene ND 0 025 A-01 Toluene ND 0 025 A-01 Ethylbenzene ND 0 025 A-01 Xylenes(total) ND 0 025 H 11 A-01,AF-13 Surrogate a,a,a-Trifluorotoluene 961 % 60-140 A-01 MW-9@60'(S109022-27)Sod Sampled 08/31/0100 00 Received 09/04/01 17 04 Purgeable Hydrocarbons 4400 200 mg/kg 40 1090111 09/11/01 09/1 I/01 DHS LUFT Benzene 77 10 " h 09/11/01 " Toluene 50 10 " Ethylbenzene 34 10 " Xyleaes(total) 210 10 09/11/01 " Surrogate a a,a-Trifluorotoluene 170% 60-140 09111101 S-02 Sequoia Analytical- Sacramento 77te results to this report apply to the samples analyzed in accordance with the chain custody document Thu analytical report must be reproduced in its entirety Page 3 of 16