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44�^.;rya <br /> Page -23- <br /> Parameter Preparation Yield <br /> f r. <br /> Trichloroethene Add 0.5 mL of 140 ug/L to 7.0 ug/L <br /> (TCL) 850 mL of sample, extract <br /> into 10 mL of hexane <br /> Total Petroleum For liquid samples - <br /> Hydrocarbons Add 0.1 mL of 8820 ug/L 41 ug/L <br /> (TPH) gasoline into 30 mL <br /> of sample, extract <br /> into 5.0 mL of <br /> carbon disulfide <br /> For solid samplee - <br /> Add 0.3 mL of 8850 ug/L 132 ug/L <br /> gasoline into 30 g <br /> of sample, extract <br /> into 20 mL of <br /> ethyl acetate <br /> EPA 624/8240 Adf 10 uL of 10 ug/L <br /> (Volatile spike solution. (or <br /> Organics) (containing 25 mg/L 10 ug/kg) <br /> of methylenechloride, <br /> trichlorofluoromethane, <br /> i,l-dichloroethene, <br /> 1,1-dichloroethane, <br /> chloroform, <br /> i carbon tetrachloride, ~. <br /> 1,2-dichloropropane <br /> trichloroethene, <br /> 1,1,2-trichloroethane, <br /> dibromochloramethane, <br /> tetrachloroethene, <br /> chlorobenzene, benzene, <br /> bromoform, <br /> 1,1,2,2-tetrachloroethane, ' <br /> toluene, ethylbenzene, <br /> trans-1,2-dichloroethene, <br /> 1,2-dichloroethane, <br /> bromodichloramethane, <br /> s trans-1,3-dichloropropene, <br /> cis-1,3-dichloropropane, <br /> chloromethane, bromomethane, <br /> vinyl chloride,chloroeth2ne, <br /> g 1,2 dichlor„benzene, <br /> +� dichloro-1,3 benzene, <br /> dichloro-1,4-benzene, <br /> m-xylene, acetone, <br /> carbon disulfide, <br /> 2-butanone, <br /> vinyl acetate, <br /> 4-methyl-2-pentanone, <br /> 2-hexanone, styrene, - <br /> 0-xylene, <br /> in methanol) to <br /> 25 mL of sample <br /> (or 25 g of solid sample). <br /> RECEIVED °tik�t i 3 'i:f <br />