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MATRIX SPIKE SAMPLE DATA REPORT GC Semivolatiles Client Lot #- - - : EOJ170165 Work Order #. . . : DM9V81AF-MS Matrix. . . . . . . . . : WATER MS Lot-Sample #:, EOJ170165-001 DM9V81AG-MSD Date Sampled. . . : 10/12/00 11:00 Date Received. . : 10/17/00 10:00 MS Run #. . . . . . . : 0297020 Prep Date- - - - - - : 10/20/00 Analysis Date. . : 10/20/00 Prep Batch #. . . : 0297143 Analysis Time. . : 14 :03 Dilution Factor: 1 SAMPLE SPIKE MEASRD PERCENT . PARAMETER AMOUNT AMT AMOUNT UNITS RECOVERY RPD METHOD Triethylene glycol ND 421 363 mg/L 86 SW846 8015B ND 421 382 mg/L 91 5.0 SW846 8015E n-Butanol ND 101 108 mg/L 107 SW846 8015B ND 101 108 mg/L 107 0 .33 SW846 8015B 2-Chloroethanol ND 119 128 mg/L 107 SW846 8015B ND 119 125 mg/L 105 2 .5 SW846 8015B Diethylene clycol ND 426 420 mg/L 98 SW846 8015E ND 426 423 mg/L 99 0.49 SW846 8015B 2-Methoxyett-:anol ND ill 116 mg/L 104 SW846 8015B ND 111 116 mg/L 105 0.22 SW846 8015B Ethylene glycol ND 412 425 mg/L _ 102 SW846 8015B ND 412 428 mg/L 102 0.73 SW846 8015B 2-Ethoxyethanol ND 109 114 mg/L 105 SW846 8015B ND 108 113 mg/L 105 0.05 SW846 8015B n-Propanol ND 115 128 mg/L 112 SW846 8015B ND 115 128 mg/L 111 0.18 SW846 8015B 1,4-Dioxane ND 112 111 mg/L 99 SW846 8015B ND 112 111 mg/L 99 0.22 SW846 8015B Diethylene glycol monobut 124 129 mg/L 104 SW846 8015B 124 129 mg/L 104 0.0 SW846 8015B ND 102 126 mg/L 124 a 1.5 SW846 801513 ND 114 129 mg/L 113 0.17 SW846 8015B NOTE(S) : Calculations are performed before rounding to avoid round-off errors in calculated results. Bold print denotes coot rol parameters a Spiked analyte recovery is outside stated control limits.