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i <br /> MATRIX SPIKE SAMPLE DATA REPORT <br /> GC/MS Volatiles <br /> Client Lot #. . : EOJ170165 Work Order #. . : DM9WVIAF-MS Matrix . . . . . . . : WATER <br /> MS Lot-Sample #: EOJ170165-006 DM9WVIAG-MSD <br /> Date Sampled. . : 10/12/00 13 10 Date Received. . : 10/17/00 10 00 MS Run #- . . . - 0305003 <br /> Prep Date. . . . : 10/21/00 Analysis Date. . : 10/21/00 <br /> Prep Batch #. 0305092 Analysis Time. . : 20 19 <br /> Dilution Factor: 50 <br /> SAMPLE SPIKE MEASRD PERCENT <br /> PARAMETER AMOUNT AMT AMOUNT UNITS RECOVERY RPD METHOD <br /> Benzene 1700 500 2130 ug/L 84 SW846 8260B <br /> 1700 500 2050 ug/L 68 a 3.9 SW846 8260B <br /> Chlorobenzene ND 500 419 ug/L 84 SW846 8260B <br /> ND 500 423 ug/L 85 0.90 SW846 8260B <br /> 1,1-Dichloroethene ND 500 430 ug/L 86 SW846 8260B <br /> ND 500 416 ug/L 83 3.4 SW846 8260E <br /> Toluene 1500 500 1950 ug/L 85 SW846 8260B <br /> 3.500 500 3.920 ug/L 78 a 1.9 SW846 8260B <br /> Trichloroethene ND 500 426 ug/L 85 SW846 8260B <br /> i <br /> ND 500 420 ug/L 84 1.4 SW846 8260B <br /> PERCENT RECOVERY <br /> SURROGATE RECOVERY LIMITS <br /> Bromofluorobenzene 98 (75 - 120) <br /> 98 (75 - 120) <br /> 1,2-Dichloroethane-d4 94 (65 - 130) <br /> 94 (65 - 130) <br /> Toluene-dS 104 (80 - 130) <br /> 104 (80 - 130) <br /> NOTE(S) : <br /> Calculations are performed before rounding to avoid found off errors in calculated results <br /> Bold print denotes control parameters <br /> a Spiked analyte recovery is outside stated control limas <br /> 000OG3 <br />