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' Q UAL I T Y C O N T R O L R E S U L T 5 <br /> Job Number 992705 Report Date 01/06/2000 <br />' CUSTOMER IT Group PROJECT- Southland - Martinez ATTN Rhonda Teicheira <br /> QC Type Description Rea, Code Lab ID Dilution Factor T Date Time <br />' MSD Matrix Spike Duplicate 09112901 992556-b 1 12/07/1999 1740 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits F <br />�1,2-Dichloroethane 9 97 11 04 10 000000 0 99 7 70-130 <br /> 10 30 <br /> 1,2-Dibromoethane (EDB) b 17 8 29 10 000000 0 61 7 70-130 X <br /> 29 30 <br /> 1 <br /> MS Matrix Spike O91207G 992636-2 12/24/1999 0225 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits F <br /> tert-Butyl Alcohol (TBA) 1161 58 1000 000000 1 80 116 0 34-182 <br /> Di-Isopropyl Ether 61 54 50 000000 0 123 1 60-131 <br /> Ethyl tert-Butyl Ether (ETRE) 57 07 50 000000 0 114 1 64-138 <br /> tert-Amyl Methyl Ether 53 84 50 000000 0 91 105 9 67-154 <br /> Methyl-t-Butyl Ether (MTBE) 141 59 100 000000 20 29 121 3 71-142 <br /> 1,2-Dichloroethane 10 26 10 000000 0 102 6 70-130 <br /> 1 -Dibromoethane (EDB) 10 77 10 000000 0 107 7 70-130 <br />' <br /> MSD Matrix Spike Duplicate 09120705 992636-2 12/24/1999 0259 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits F <br /> 1 tert-Butyl Alcohol (TBA) 982 02 1161 58 1000 000000 1 80 98 0 34-182 <br /> 17 19 <br /> D1-Isopropyl Ether 55 30 61 54 50 000000 0 110 6 60-131 <br /> 11 24 <br />' Ethyl tert-Butyl Ether (ETBE) 52 73 57 07 50 000000 0 105 5 64-138 <br /> 8 29 <br /> tent-Amyl Methyl Ether 51 98 53 84 50 000000 0 91 102 1 67-154 <br /> 4 27 <br />'Methyl-t-Butyl Ether (MTBE) 121 56 141 59 100 000000 20 29 101 3 71-142 <br /> 15 31 <br /> 1,2-Dichloroethane 9 90 10 26 10 000000 0 99 0 70-130 <br /> 4 30 <br />' 1,2-Dibromoethane (EDB) 9 18 10 77 10 000000 0 91 8 70-130 <br /> 16 30 <br />' LCS Laboratory Control Sample 09123101 1 01/04/2000 0636 <br /> Parameter/Test Description QC Result OC Result True Value Orig Value Calc Result * Limits F <br /> tert-Butyl Atcohol (TBA) 1090 83 1000 000000 109 1 37-175 <br />'Di-Isopropyl Ether 48 73 50 000000 97 5 60-138 <br /> Ethyl tert-Butyl Ether (ETRE) 52 59 50 000000 105 2 51-143 <br /> tert-Amyl Methyl Ether 49 15 50 000000 98 3 54-137 <br /> Methyl-t-Butyl Ether (MTBE) 97 57 100 000000 97 6 33-169 <br />' 1,2-Dichloroethane 9 96 10 000000 99 6 70-130 <br /> 1,2-Dibromoethane (EDB) 9 92 10 000000 99 2 70-130 <br /> Page 11 * %=% REC, R=RPD, A=ABS Diff D=X Diff <br />