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i <br /> COULAB CORE LABORATORIES <br /> Q UAL i T Y C O N T R O L R E S U L T S <br /> Job Number 990890 Report Date 05/26/1999 <br /> CUSTOMER: IT Group PROJECT- Southland - Martinez ATTrl, Shelby Lathrop <br /> QC Type Description Reag Code--'7 Lab ID Dilution Factor Date Time <br /> ' LCS tabpratory Control Sample 09059803 05/25/1999 1031 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits <br /> ethyl-t-Butyl Ether (MTBE) 84 19 100 000000 84 2 70-130 <br /> ,2-Dichtoroethane 8 58 10 000000 85 8 70-130 <br /> 1,2-Dtbromoethane (EDB) 8 11 10 000000 81 1 70-130 <br /> tMS Matrix Spike 09051803 990881-3 05/2511999 1130 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits <br /> lert-ButyL Alcohol (TBA) 942 52 1000.000000 fl 94 3 70-130 <br /> i-Isopropyl Ether 46 10 50 000000 0 92 2 70-130 <br /> Ethyl tert-Butyl Ether (ETRE) 45 41 50 000000 0 90 8 70-130 <br /> tert-Amyl Methyl Ether 47 71 50 000000 0 95 4 70-130 <br /> 9ethyl-t-Butyl Ether (MTBE) 98 48 100 000000 0 98 5 70-130 <br /> ,2-Dichloroethane 10 43 10 000000 0 104 3 70-130 <br /> ,2-Dibromoethane (EDB) 10 18 10 000000 0 101 8 70-130 <br /> 1W:=EM---3tr-,xsp- <br /> ke Duplicate 09051803 990881-3 05/25/1999 1159 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits <br /> ert-Butyl Alcohol (TBA) 1083 56 942 52 1000 000000 0 108 4 70-130 <br /> 14 25 <br /> Ki-isopropyL Ether 51 68 46 10 50 000000 0 103 4 70-130 <br /> 11 25 <br /> thyl tert-Butyl Ether (ETRE) 51 04 45 41 50 000000 0 102 1 70-130 <br /> 12 25 <br /> ert-Amyl Methyl Ether 51 33 47 71 50 000000 0 102 7 70-130 <br /> 7 25 <br /> Methyl-t-Butyl Ether (MTBE) 110 90 98 48 100 000000 0 110 9 70-130 <br /> 12 25 <br /> 11 <br /> 2-Dichloroethane 10 98 10 43 10 000000 0 109 8 70-130 <br /> 5 25 <br /> 1,2-Dtbromoethane (EDB) 10 24 10 18 10 000000 0 102 4 70-130 <br /> 1 25 <br /> Test Method EPA 8260B Batch - 6417 Analyst vz <br /> Method Description Volatile Organics by GC/MS Units ug/L <br /> MS Matrix Spike 09051803 990876-23 05/24/1999 1411 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits <br /> ert-Butyl Alcohol (TBA) 998 53 1000 000000 0 99 9 70-130 <br /> t-Isopropyl Ether 50 76 50 000000 0 101 5 70-130 <br /> Ethyl tert-Butyl Ether (ETRE) 48 23 50 000000 0 96 5 70-130 <br /> fe r t-Amy <br /> l Methyl Ether 48 91 50 000000 0 97 8 70-130 <br /> ett-t-Butyl Ether (MTBE) 84 31 100 000000 0 83 83 5 70-130 <br /> 2-Dichloroethane 8 13 10 000000 0 81 3 70-130 <br /> ibromoethane (EDB) 9 14 10 000000 0 91 4 70-130 <br /> ' Page 8 <br /> * %=Y REC, R=RPD, A=ABs Diff D=7 Diff <br /> rno an yl rs vs us on t ie.a welo uro la n�1 eoo I olse<f ulnn pro malwn�nll 1 n8ouliol cl Irt wi o�ry d a eco Ib n,I n sl li 9 >,v Illasn nwI 11 n lylen wns ou o 1 1 I to <br /> wess d c�1 rw Dene 13 eni of eo n�awt nl mee roew n�wl�rn swore o tk«s 1 w n Ito I�r 1 a on.a 1 onruu en of>>v Irl In 1 Isn tc 1 �anoia w 11 are o<e 1 1 11 nl J nlnv o 1 e ioi c r <br /> of 4 s u�xltY wNla v 5e1Jm It Ou Ih IqI o1 Gf w1 v lII w 111 IC <br />