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CGeo(aguaL2ecFinus Znc • Page 3 <br /> Valentine(Castle Motors) <br /> Vertical Def AT <br /> August 23, 2000 <br />' • Benzene, toluene, ethylbenzene and xylene (BTEX) by EPA method 8020 <br /> • Gasoline range petroleum hydrocarbons (TPH-Gas) by EPA method 5030/8015(m) <br /> • Methyl Tertiary Butyl Ether (MTBE) by EPA method 8020 <br />' • In addition, two soil samples wt11 be analyzed for the fuel oxygenate suite (MTBE, DIPE, <br /> ETBE, TAME & TBA) by EPA method 8260 <br /> The detection limits for these compounds are listed below A Chain of Custody will be <br /> completed for all samples collected and tracked to ensure sample integrity <br /> Ethers _ <br /> Detection Limits 8020 8260 EDB 8260 8015m <br /> Soil (µg/Kg) 30 5 50 20 1,000 <br /> 2.2 Soil & Pore Water Sample Collection with the SimulProhe <br />' When intervals are detected that are suitably coarse grained, attempts will be made to collect P <br /> pore water samples using the SimulProbe sampling tool <br />' The SimulProbe allows a pore water sample to be collected at the exact interval from which a <br /> soil sample is collected thus providing correlative information on the sorbed portion of the <br /> contaminated zone Furthermore, the SimulProbe's design reduces the possibility of cross <br /> contamination from shallower borehole waters <br /> After the SimulProbe groundwater sampling tool is advanced into the saturated zone, the tool <br /> is retracted to expose the screen The sample collection chamber is allowed to fill under <br />' ambient hydrostatic pressure Once full the chamber is sealed with a pneumatically actuated <br /> (N2 gas) solenoid valve and the apparatus is brought to the surface The sample chamber is <br /> carefully emptied using a bottom-emptying device thus reducing the possibility of sample ' <br />' agitation and volatilization Once the sample container (40-m1 VOA) is filled and capped, <br /> the bottle will be inverted, tapped, and checked for headspace bubbles The sample container <br /> is identified and labeled with a unique designation, inserted into foam holders and placed in <br /> an ice chest cooled to 40C for transport to the laboratory <br />' Once the borehole has extended below groundwater, pore water samples will be collected at <br /> geologically significant units using the SimulProbe It should be rioted that collection of pore <br />' water samples might not be successful 1n clay units <br /> 2.2.1 Soil & Pore Water Sample Analysis <br />' Up to five samples of soil-pore water from MW-201 will be submitted to CLS Laboratories <br /> (State Certified Laboratory #1233) Samples will be analyzed for the following <br /> • Benzene, toluene, ethylbenzene and xylene (BTEX) by EPA method 8020 <br /> • Gasoline range petroleum hydrocarbons (TPH-Gas) by EPA method 5030/8015(rn) <br /> • Fuel oxygenate suite (MTBE, DIPE, ETBE, TAME & TBA) by EPA method 8260 <br /> • 1,2-DCA, EDB, Methanol, & Ethanol by method 8260 <br /> The detection limits for these compounds are listed below A Chain of Custody will be <br /> completed for all samples collected and tracked to ensure sample integrity <br />