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M <br /> Entech Analytical Labs, Inc., Santa Clara, CA <br /> Lab Report No.: H2121801 Date: 12/27/2002 Page: 1 <br /> Project Name: VALENTINE/CASTLE Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: 429490J Method: 8260FA <br /> Prep Meth: SW5030B <br /> LField ID: MW-201 Lab Samp ID: 32599-001 <br /> Deser/Location: MW-201 Recd Date: 12/18/2002 <br /> Sample Date: 12/17/2002 Prep Date: 12/1912002 <br /> I <br /> tSample Time: 1315 Analysis Date: 12/19/2002 <br /> Matrix: Water QC Batch: WMS11850 <br /> Basis: Not.Filtered Notes: M <br /> Lr <br /> Analyte Det Limit Rep Limit Note Result Units 'Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 0.3 1. PQL ND UG/L 1 <br /> L Ethyl tert-butyl ether(ETRE) 0.5 5. PQL ND UG/L 1 <br /> tent-Amyl methyl ether(TAME) 0.3 S. PQL ND UG/L 1 <br /> Di-isopropyl ether(DIPE) 0.5 5. PQL ND UG/L 1 <br /> Ltent-Butyl alcohol (TBA) 4.6 10. PQL ND UG/L 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> 4-Bromofluorobenzene 65-135 SMEA 119.0% 1 <br /> Toluene-d8 77-150 SMEA 115.0% 1 <br /> Dibromofluoromethane 57-156 SMEAAZ 4.6% 1 1 <br /> ' . AZ: Surr. recovery outside of acceptance limits due to matrix intert. <br /> { <br /> l <br /> 1 <br /> 5 � ` <br /> �. <br /> Approved by:�t�! Date: I��.6 <br /> I L ! <br /> j <br />