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S <br /> Entech Analytical Labs, Inc , Santa Clara, CA <br /> Lab Report No H2O22801 Date 03/06/2002 Page 7 <br /> Protect Name VALENTINE Analysis Volatile Organic Compounds by GC/MS Fuel <br /> Project No 7232 Method 8260FA <br /> Prep Meth SW5030B <br /> ' Field ID MW-5 Lab Samp ID 29086-001 <br /> Descr/Location MW-5 Recd Date 02/28/2002 <br />' Sample Date 02/27/2002 Prep Date 03/01/2002 <br /> Sample Time 0930 Analysis Date 03/01/2002 <br /> Matrix Water QC Batch WMS31450 <br />' Basis Not Filtered Notes SH <br /> Analyte Det Limit Rep Limit Nate Result Units Pvc Dil <br /> Methyl-cert-butyl ether (MTBE) 15 250 PQL ND UG/L 50 <br /> tert-Butyl ethyl ether(ETBE) 25 250 PQL ND UG/L 50 <br /> tert-Amyl methyl ether(TAME) 15 250 PQL ND UG/L 50 <br />' Di-isopropyl ether(DIPE) 25 250 PQL ND UG/L 50 <br /> tert-Butyl alcohol (TBA) 550 1000 PQL. ND UG/L 50 <br /> 1,2-Dichloroethane 15 250 PQL ND UGIL 50 <br />' 1,2-Dibromoethane 25 250 PQL ND UG/L 50 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> 4-Bromofluorobenzene 65-135 SMSA 85% # <br /> Toluene-d8 77-150 SMEA 110% 1 <br /> Dibromofluoromethane 57-156 SMEA 99% 1 <br /> BH Reporting limits raised due to high level of non-target analytes <br /> 1 <br /> 1 <br /> ApprOVea Dy Uate �� �' <br />