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Entech Analytical Labs, Inc , Santa Clara, CA <br /> Lab Report No H2022801 Date 03/06/2002 Page 2 <br /> ' Protect Name VALENTINE Analysis Volatile Organic Compounds by GC/MS Fuel <br /> Protect No 7232 Method 8260FA <br /> Prep Meth SW5030B <br /> ' Field ID MW-101 Lab Samp ID 29086-004 <br /> Descr/Location MW-101 Recd Date 02/28/2002 <br /> Sample Date 02/27/2002 Prep Date 03/01/2002 <br /> Sample Time 1101 Analysis Date 03/01/2002 <br /> Matrix Water QC Batch WMS31450 <br /> Basis Not Filtered Notes <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tent-butyl ether(MTBE) 03 5 PQL ND UGIL 1 <br /> tent-Butyl ethyl ether(ETRE) 05 5 PQL ND UGIL 1 <br /> tert-Amyl methyl ether (TAME) 03 5 PQL NO UG/L 1 <br /> Di-isopropyl ether(DIPE) 05 5 PQL ND UGIL 1 <br /> tert-Butyl alcohol (TBA) 11 20 PQL ND UGIL 1 <br /> 1,2-Dichloroethane 03 5 PQL ND UG/L 1 <br /> 1,2-Dibromoethane 05 5 PQL ND UG/L 1 <br /> ' SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> 4-Bromotluorobenzene 65-135 SMSA 83% 1 <br /> Toluene-d8 77-150 SMEA 108% 1 <br /> Dibromofluoromethane 57-156 SMEA 100% 1 <br /> r <br /> r <br /> Approved by Ovate <br /> ��tU� <br />