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1 <br /> Entech Analytical Labs, Inc . Santa Clara, CA <br /> 1 Lab Report No H2O22801 Date 03/06/2002 Page 6 <br />' Protect Name VALENTINE Analysis Volatile Organic Compounds by GC/MS Fuel <br /> Project No 7232 Method 8260FA <br /> Prep Meth SW5030B <br />' Field ID MW-4 Lab Samp ID 29086-006 <br /> Descr/Location MW-4 Rec'd Date 02/28/2002 <br /> Sample Date 02/27/2002 Prep Date 03101/2002 <br /> Sample Time 1149 Analysis Date 03/01/2002 <br /> Matrix Water QC Batch WMS31450 <br /> Basis Not Filtered Notes <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> 1 Methyl-tent-butyl ether(MTBE) 03 5 PQL ND UG/L 1 <br /> tert-Butyl ethyl ether(ETBE) 05 5 PQL ND UG/L 1 <br /> tent-Amyl rnethyl ether(TAME) 03 5 PQL ND UG/L 1 <br /> 1 Di-isopropyl ether(DIPE) 05 5 PQL ND UG/L 1 <br /> tent-Butyl alcohol (TBA) 11 20 PQL ND UG/L 1 <br /> 1,2-Dichloroethane 03 5 PQL ND UG/L 1 <br /> 1,2-Dibromoethane 05 5 PQL NO UG/L 1 <br /> 1 SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> 4-8romotluorobe nzene 65-135 SMEA 87% 1 <br /> Toluene-d8 77-150 SMEA 102% 1 <br /> Dibromofluoromethane 57-156 SMEA 99% 1 <br /> 1 <br /> i <br /> 1 <br /> 1 <br /> 1 <br /> 1 <br /> Approved ay __ I -—— Uate <br />