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Entech Analytical Labs, Inc , Santa Clara, CA <br /> Lab Report No H1121205 Date 12/26/2001 Page 7 <br /> Protect Name CASTLE MOTORS Analysis Volatile Organic Compounds by GC/MS Fuel <br /> Project No 7232 Method 8260FA <br /> Prep Meth SW5030B <br /> ' Field ID MW-5 Lab Samp ID 28164-001 <br /> Deser/Location MW-5 Rec'd Date 12/13/2001 <br /> Sample Date 12/11/2001 Prep Date 12/20/2001 <br /> Sample Time 0815 Analysis Date 12/20/2001 <br /> Matrix Water QC Batch WMS11325 <br /> Basis Not Filtered Notes <br /> Analyte Det Limit Rep Limit Note Result Units <br /> Pvc Dil <br /> Methyl-tert-butyl ether 3 50 PQL NO UG/L 10 <br /> ' tert-Butyl ethyl ether 5 50 PQL NO UGIL 10 <br /> tert-Amyl methyl ether 3 50 PQL ND UG/L 10 <br /> Di-isopropyl ether(DIPS) 5 50 PQL NO UGIL 10 <br /> ' tert-Butyl alcohol 110 200 PQL NO UG/L 10 <br /> 1,2-Dichloroethane 3 50 PQL ND UGIL 10 <br /> 1,2-ā¯‘ibromoethane 5 50 PQL ND UGIL 10 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> 4-8romofluorobenzene 65-135 SMSA 99% 1 <br /> Toluene-d8 65-135 SMEA 108%Alkil 1 <br /> Dibromofluoromethane 57-139 SMSA 107% 1 <br /> 1 <br /> Approvea t)y Uate <br /> 1 <br />