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i i i i i i ii i i i i i l ir i <br /> QAIQ�epart <br /> Matrix Spike/Duplicate Matrix Spike Summary <br /> Castle Analytical Laboratory, Atwater, CA <br /> Lab Report No H3091604 Date 09/22/2003 Page 17 <br /> QC Batch VWMS-9173 Protect Name Lab Generated or Non COE Sample <br /> Matnx Water Protect No Lab Generated or Non COE Sample <br /> Lab Samp ID VWMS-9173 Field ID Lab Generated or Non COE Sample <br /> Basis Not Filtered Lab Ref ID 6073-1 WQ <br /> Acceptance <br /> Analysis Spike Level Sample Spike Result % Recoveries Criteria <br /> Analyte Method MS DMS Result MS DMS Units MS DMS RPD % Ree RPD <br /> 1,2-Dibromoethane 8260FA 25 25 010 281 265 UGIL 108 102 57 127-76 MSA 201VISP <br /> 1,2-Dichloroethane 8260FA 25 25 011 284 258 UGIL 109 988 98 124-70 MSA 20 LSP <br /> Di-isopropyl ether(DIPE) 8260FA 25 25 006 292 257 UGIL 114 100 13 151-51 MSA 201-SP <br /> Ethyl tert-butyl ether(ETRE) 8260FA 25 25 005 287 254 UGIL 113 996 13 138.57 MSA 201-SP <br /> Methyl-tert-butyl ether(MTBE) 8260FA 25 25 034 246 232 UGIL 848 792 68 127-62 MSA 20LSP <br /> tent-Amyl methyl ether(TAME) 8260FA 25 25 CLI 1 2 87 254 UGIL 110 972 12 122-60 MSA 201-SP <br /> tert-Butyl alcohol(TBA) 8260FA 750 750 465 6566 6464 UGIL 813 800 16 168-42 MSA 20LSP <br /> 1,2-Dichloroethane-d4 8260FA 100 100 1051 91 7 873 PERCENT 917 873 49 141-63 SMSA 205MSP <br /> Toluene-dB 8260FA 100 100 1053 96 9 94 2 PERCENT 96 9 94 2 2 B 129 76 SMSA 20SMSP <br /> I <br />