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Excelchem Environmental Labs, Roseville, CA <br /> ' Lab Repo;;i No 0502016 Date 03/02/2005 Page 5 <br /> ' Protect Name CASTLE MOTORS Analysis Volatile Organic Compounds by GC/MS <br /> Protect No NA Method SW8260B <br /> Prep Meth SW5030 <br /> ' Field ID MW-109 Lab Samp ID 0502016-16 <br /> Descr/Location MW-109 Rec'd Date 02/04/2005 <br /> ' Sample Date 02/01/2005 Prep Date 02/09/2005 <br /> Sample Time 1328 Analysis Date 02/09/2005 <br /> Matrix Water QC Batch 0102058260 <br /> ' Basis Not Filtered Notes <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> ' Benzene 05 05 PQL ND UG/L 1 <br /> 1,2-Dibromoethane 05 05 PQL ND UG/L 1 <br /> 1,2-Dichloroethane 05 0 5 PQL ND UG/L 1 <br /> Ethylbenzene 05 05 PQL ND UG/L 1 <br /> Toluene 05 05 PQL ND UG/L 1 <br /> o-Xylene 05 05 PQL ND UG/L 1 <br /> Methyl-tert-butyl ether (MTBE) 05 05 PQL ND UG/L 1 <br /> Di-isopropyl ether(DIPS) 05 05 PQL ND UG/L 1 <br /> Ethyl tert-butyl ether (ETBE) 05 05 PQL ND UG/L 1 <br /> Gasoline Range Organics 50 50 PQL ND UG/L 1 <br /> tert-Amyl methyl ether (TAME) 05 05 PQL ND UG/L 1 <br /> tent-Butyl alcohol (TBA) 50 50 PQL ND UG/L 1 <br /> ' Xylene, Isomers m & p 10 10 PQL ND UG/L 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> 4-B.omofluorobenzene 70-130 SLSA 94% 1 <br /> ' Toluene-d8 70-130 SLSA 96% 1 <br /> Dibromofluoromethane 70-130 SLSA 97% 1 <br /> 1 <br /> 1 <br />' Approved by Date ^o <br />