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Excelchem Environmental Labs, Roseville, CA <br /> ' Lab Report No 0502016 Date 03/02/2005 Page 11 <br /> ' Project Name CASTLE MOTORS Analysis Volatile Organic Compounds by GC/MS <br /> Project No NA Method SW8260B <br /> Prep Meth SW5030 <br /> Field ID MW-3 Lab Samp ID 0502016-03 <br /> Descr/Location MW-3 Rec'd Date 02/04/2005 <br /> ' Sample Date 01/27/2005 Prep Date 02110/2005 <br /> Sample Time 1329 Analysis Date 02/10/2005 <br /> Matrix Water QC Batch 0102058260 <br /> ' Basis Not Filtered Notes <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> ' Benzene 500 500 PQL 14000. UG/L 1000 <br /> 1,2-Dibromoethane 500 500 PQL ND UGIL 1000 <br /> 1,2-Dichloroethane 500 500 PQL ND UGIL 1000 <br /> ' Ethylbenzene 500 500 PQL 2300. UGIL 1000 <br /> Toluene 500 500 PQL 21000. UGIL 1000 <br /> o-Xylene 500 500 PQL 3900. UGIL 1000 <br /> ' Methyl-tert-butyl ether (MTBE) 500 500 PQL ND UGIL 1000 <br /> Di-isopropyl ether(DIPE) 500 500 PQL ND UGIL 1000 <br /> Ethyl tert-butyl ether (ETBE) 500 500 PQL ND UG/L 1000 <br /> Gasoline Range Organics **"* **** PQL Cl 96000 UGIL 1000 <br /> tert-Amyl methyl ether(TAME) 500 500 PQL ND UGIL 1000 <br /> tert-Butyl alcohol (TBA) 5000 5000 PQL ND UGIL 1000 <br /> ' Xylene, Isomers m & p 1000 1000 PQL 8000. UGIL 1000 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> 4-Bromofluorobenzene 70-130 SLSA 98% 1000 <br /> Toluene-d8 70-130 SLSA 97% 1000 <br /> Dibromofluoromethane 70-130 SLSA 95% 1000 <br /> CI See narrative <br /> 1 <br /> 1 <br /> 1 <br />' Approved by _ Date —e <br />