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PRECISION <br /> ENVIRO-TECH <br /> Analytical Laboratory CERTIFICATE OFANALYSIS <br /> Tuesday,March 29,2005 <br /> Attention: Jack Bishop <br /> California Tank Lines Report Page 18of21 <br /> P O BOX 6245 <br /> Stockton, CA 95266 <br /> Volatile Organic Compounds by EPA Method 8260B- Quality Control <br /> Precision Enviro-Tech <br /> Reportmg Spike Source %REC RPD <br /> [Amiyte Result Linut Units Level Result V*REC Lmuts RPD Lxmzt Notes <br /> Batch AC51507-Volateles <br /> Matrix Spike(AC51507-MSI) Source 5031206-01 Prepared 15-Mar-05 Analyzed 16-Mar-05 <br /> m,p-Xylene 486 0 500 ugll 400 ND 122 75-122 <br /> "-Xylene 236 0 500 200 ND 118 75-122 <br /> Matnx Spike Du (AC51507-MSDI) Source 5031206-01 Prepared 15-Mar-05 Analyzed 16-Mar-05 <br /> Methyl tert-butyl Ether(MtBE) 185 0 500 ug/l 200 ND 92 75-122 1 15 <br /> Dusopropyl Ether(DIPE) 166 0 500 200 ND 83 75-122 3 15 <br /> Ethyl tert-Butyl Ether(ETBE) 184 0 500 " 200 ND 92 75-122 3 15 <br /> tert-Amyl Methyl Ether(TAME) 197 0 500 200 ND 98 75-122 14 15 <br /> Benzene 208 0 500 200 ND 104 75-122 6 15 <br /> (benzene 204 0 500 200 ND 102 75-122 8 15 <br /> ne 239 0 500 200 ND 120 75-122 4 15 <br /> m,p-Xylene 426 0 500 400 ND 106 75-122 13 15 <br /> o-Xylene 210 0 500 200 ND 105 75-122 12 15 <br /> mg/L=milligrams per Liter=ppm DLR=Detection Lima for Purpose of Reporting <br /> rTIL=micrograms per Liter=ppb Fxceptional sample matrices or interferences may <br /> result to higher detection limitsSPECTFULLY SUBMITTED, <br /> ��-5/OLIZ� <br /> Jonathan Le,Laboratory Director <br /> 7743 N West Lane Suite B2 Stockton CA 95210 phone (209) 477-8105 Fax (209) 477-8148 <br />