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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> bttiii//www rnccamnbell com E-mail main@mccampbell coin <br /> ' Advanced GeoEnvironmental Client Project ID Pacific Pride/S El Date Sampled 07/24/01 <br /> � <br /> 837 Shaw Road Dorado Date Received 07/25/01 <br /> ' Stockton,CA 95215 Client Contact Tim Cucllar Date Extracted 07/25/01 <br /> Client P 0 Date Analyzed 07/27/01 <br /> ' Diesel Range(C10-C23)and Oil-Range(C18+)Extractable Hydrocarbons as Diesel and Motor Oil* <br /> EPA methods modified 8015,and 3550 or 3510,California RWQCB(SF Bay Region)method GCFID(3550)or GCFID(3510) <br /> Lab ID Client ID Matrix TPH(d)+ TPH(mo)+ %Recovery <br /> Surrogate <br /> 73284 P-5140-50 W ll0,d,i ND 103 <br /> ' 73285 P-5170-80 W ND ND 102 <br /> 73286 P-5195-105 W ND ND 102 <br /> ' 73287 P-51120-125 W 330,d,i ND 115 <br /> 73288 SP-I S 6 9,g 34 102 <br /> 73289 SP-2 S 5 5,g,b 19 101 <br /> 73290 SP-3 S 8 6,g 33 102 <br /> i <br /> 1 <br /> Reporting Limit unless otherwise W 50 ug/L 250 ug/L <br /> stated,ND means not detected above <br /> ' the reporting limit S 10 mg/kg 5 0 mg/kg <br /> *water samples are reported in ug/L,wipe samples in ug/wipe,soil and sludge samples in mg/kg,and all TCLP I STLC I SPLP extracts in <br /> ug/L <br /> C cluttered chromatogram resulting in coeluted surrogate and sample peaks,or,surrogate peak is on elevated baseline,or,surrogate has been <br /> dirrunished by dilution of original extract <br /> +The following descriptions of the TP11 chromatogram are cursory in nature and McCampbell Analytical is not responsible for their <br /> interpretation a)unmodified or weakly modified diesel is significant,b)diesel range compounds are significant,no recognizable pattern,c) <br /> aged diesel's is significant),d)gasoline range compounds are significant,e)medium boiling point pattern that does not match diesel (9),f) <br /> one to a few isolated peaks present, g)oil range compounds are significant,h)lighter than water imirnscible sheen is present, i) Liquid <br /> sample that contains greater than—5 vol %sediment. <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />