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1 <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//wwwrnccampbcl1com E-mail main@mccampbell com <br /> I I <br /> Advanced GeoEnvironmental Client Project ID Pacific Pride/S El Date Sampled 07/24/01 <br /> 837 Shaw Road Dorado Date Received 07/25/01 <br /> Stockton,CA 95215 Client Contact Tori Cuellar Date Extracted 07/27-07/30/01 <br /> Client P O Date Analyzed 07/27-07/30/01 <br /> Seven Oxygenated Volatile Organics By GUMS <br /> EPA method 8260 modified <br /> 1 Lab ID 73288 73289 73290 <br /> Reporting Limit <br /> Client ID SP-1 SP-2 SP-3 <br /> ' Matrix S S S S w <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPS) ND ND ND 50 10 <br /> ' Ethyl tert-Butyl Ether(ETRE) ND ND ND 50 10 <br /> Methyl-tert Butyl Ether(MTBE) NO ND ND 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND 50 10 <br /> tert-Butanol ND ND ND 25 50 <br /> ' Methanol ND ND ND 1000 200 <br /> ' Ethanol ND ND ND 250 50 <br /> Surrogate Rcaivenes(%) <br /> ' Dibromotluoromethane 96 96 95 <br /> Comments <br /> 'water samples are reported in ug/L,soil and sludge samples in uglkg,wipes in ug/wipe and all TCLP/STLC/SDLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water imrmscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />