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110 2nd Avenue South, ,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax':925-798-1622 <br /> 1JW://www.mccamj2bcl1.com E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID:Martini Auto Date Sampled: 03/16/00 <br /> 4005 North Wilson Way Date Received: 03/18/00 <br /> Stockton, CA 95205 Client Contact: Bill Little Date Extracted: 03/21-03/23/00 <br /> Client P.O: Date Analyzed: 03/21-03/23/00 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> :'Lab ID 33435 <br /> Client ID 134-5 i. <br /> :Matrix S <br /> Compound ;i Concentration* Compound Concentration* <br /> Acetone @+ NDQS trans-1,3-Dichloropropene ND <br /> Benzene ND Ethylene dibromide ND <br /> Bromobenzene ND Ethylbenzene ND <br /> Bromochloromethane ND Hexachlorobutadiene ND <br /> Bmmodichloromethane ND lodomethane ND <br /> Bromoform ND Isopropylbenzene ND <br /> Bromomethane ND p-lsopropyl toluene ND <br /> n-Butyl benzene - ND Methyl butyl ketone" ND <br /> sec-Butyl benzene 3 ND Methylene Chloride"' ND <br /> tert-Butyl benzene ND Methyl ethyl ketone ND <br /> Carbon Disulfide ND Methyl isobutyl ketone"' ND <br /> Carbon Tetrachloride ND Methyl tert-Butyl Ether(MTBE) -- <br /> Chlorobenzene ND Naphthalene ND i <br /> Chloroethane ND n-Propyl benzene ND + <br /> 2-Chloroethyl Vinyl Ether" ND Styrene PT ND <br /> Chloroform ND 1,1,1,2-Tetrachlorocthane ND <br /> r Chloromethane ND 1,1,2,2-Tetrachloroethane ND <br /> 1 2-Chlorotoluene 1, ND Tetrachloroethene ND <br /> ffrr�� 4-Chlorotoluene ND Toluene- ND <br /> Dibromochloromethane ND 1,2,3-Trichlorobenzene ND <br /> 1,2-Dibromo-3-chloropropane ND 1,2,4-Trichlorabenzene ND ' <br /> Dibromomethane .; ND 3,1,1-Trichloroethane ND <br /> 1,2-Dichlorobenzene ND 1,1,2-Trichloroethane ND <br /> 1,3-Dichlorobenzene ND Trichloroethene ND <br /> 1,4-Dichlorobenzene ND Trichlorofluoromethane ND <br /> Dichlorodifluoromethane ND 1;2,3-Trichloropropane ND <br /> l,]-Dichloroethane ND 1,2,4-Trimethylbenzene ND <br /> 1,2-Dichloroethane ND 1.3,5-Trimethylbenzene ND <br /> 1,1-Dichloroethene ND Vinyl Acetate 10 ND <br /> cis-1,2-Dichloroethene ND Vinyl Chloride`03 ND <br /> trans-],2-Dichloroethene ND Xylenes,total `P ND <br /> 1,2-Dichloropropane ND Comments; <br /> 1,3-Dichloropropane ND Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND DibromoflUOTOmethane 96 <br /> 1,1-Dichloropropene ND Toluene-0 93 <br /> cis-i,3-Dichloropropene i� ND 4-BTomofluorobenzene - 106 <br /> 'water and vapor samples.are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated:water samples 1 uglL;vapor samples 0.5 ug/L;solid and sludge samples 5 ug/kg;x%�pes 0.2ug/wipe <br /> ND means not detected above the reponing limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimeihyl ketone; (c) (2-cMoroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h) lighter than water immiscible sheen is present; (i)liquid sample that contains greater than .-5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br /> . v <br />