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MATRIX SPIRE SAMPLE EVALUATION REPORT <br /> GC/MS Semivolatiles <br /> Client Lot #. ..: G41020177 Work Order #...: GPGGMIAH-MS Matrix......... SOLID <br /> MS Lot-Sample #: G4I020177-001 GPGGMIAJ-MSD <br /> Date Sampled...: 08/31/04 Date Received__: 09/02/04 <br /> Prep Date......: 09/10/04 Analysis Date..: 09/15/04 <br /> Prep Batch #._.: 4254281 <br /> Dilution Factor: 1 t Moisture._._.: 6.0 <br /> PERCENT RECOVERY RPD <br /> PARAMETER RECOVERY LIMITS RPD LIMITS METHOD <br /> Acenaphthene 84 (54 - 103) SW846 8270C <br /> 84 (54 - 103) 0.67 (0-20) SW846 8270C <br /> Pyrene 95 (39 - 126) SW846 8270C <br /> 89 (39 - 126) 5.8 (0-34) SW846 8270C <br /> 4-Chloro-3-methylphenol 90 (61 - 101) SW846 8270C <br /> 78 (61 - 101) 14 (0-32) SW846 8270C <br /> 2-Chlorophenol 79 (54 - 94) SW846 8270C <br /> 77 (54 - 94) 2.2 (0-20) SW846 8270C <br /> 1,4-Dichlorobenzene 68 (50 - 90) SW846 8270C <br /> 66 (50 - 90) 3.4 (0-51) SW846 8270C <br /> 2,4-Dinitrotoluene 90 (63 - 111) SW846 8270C <br /> 85 (63 - 111) 5.5 (0-27) SW846 8270C <br /> 4-Nitrophenol 74 (36 - 128) SW846 8270C <br /> 66 (36 - 128) 11 (0-30) SW846 8270C <br /> N-Nitrosodi-n-propyl- 77 (51 - 94) SW846 8270C <br /> amine <br /> 72 (51 - 94) 7.6 (0-68) SW846 8270C <br /> Pentachlorophenol 77 (32 - 105) SW846 8270C <br /> 64 (32 - 105) 18 (0-20) SW846 8270C <br /> Phenol 82 (55 - 95) SW846 8270C <br /> 79 (55 - 95) 4.0 (0-20) SW846 82700 <br /> 1,2,4-Trichloro- 75 (51 - 91) SW846 82700 <br /> benzene <br /> 72 (51 - 91) 4.1 (0-20) SW846 8270C <br /> PERCENT RECOVERY <br /> SURROGATE RECOVERY LIMITS <br /> 2-Chlorophenol-d4 78 (40 - 92) <br /> 77 (40 - 92) <br /> 1,2-Dichlorobenzene-d4 69 (32 - 93) <br /> 69 (32 - 93) <br /> 2-Fluorobiphenyl 82 (44 - 106) <br /> 81 (44 - 106) <br /> 2-Fluorophenol 75 (34 - 99) <br /> 78 (34 - 99) <br /> Nitrobenzene-d5 68 (37 - 89) <br /> 67 (37 - 89) <br /> (Continued on next page) <br /> G4020177 STL-Sacramento(916)373-5600 32 of 33 <br />