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+ CfI�I �O� l�C,C Irk CERTIFICATE OF ANALYSIS <br /> kr& Analytical Laboratory <br /> Frirfa)� October 15, 1499 <br /> TO: William Little <br /> Advanced GeoEnvironmental, <br /> rf 4005 N. Wilson Way <br /> Stockton, Ca. 95205 <br /> s <br /> Sample Irtfor•matiou <br /> Sample ID: PE6167-01 <br /> Sample Type: Grab <br /> ` <br /> Sample Descr•i tion: TK 1 N <br /> r.:.�. 1 P Project Nance: Quick&Save 7200 S.E1doCI) <br /> g Date/Time Sampled: 10/13/99 11:40:00 AM <br /> p Sample Matrix: Wast Water <br /> ' AI CREPORT <br /> - ANALYTICAL RESULT Q <br /> Date LCS Spike MS Spike <br /> Test-Pa1•ameter Method DLR Unit Result Analyzed Blank, Colic. LCS% Conc. MS% MSD RSD% <br /> a TPH-Gasoline EPA 8015M/DHS 1 mg/Kg ND 13-Oct-99 ND 500 112.0% 500 96.0%° 98.0% 0.5% <br /> Methyl t-Butyl Ether(MtBE) EPA8260 5 ug/Kg ND 13-Oct-99 ND 70 114.3% 70 114.3% 125.7%. 2:4% <br />;FS Diisopropyl other(DIPE) EPA8260 5 ug/Kg ND 13-Oct-99 ND 70 107.1% 70 117.1% 125.7% 1.8% <br /> Ethyl-t-butyl ether(ETRE) EPA8260 5 uglKg ND 13-Qct-99 ND 70 102.9% 70 107.1% 110.0% 0.7% <br /> ;. <br /> Tert-amyl methyl ether(TAME) EPA8260 5 ug/Kg ND 13-Oct 99 ND 70 101.4% 70 11D.0% 111.4% 0.3% <br /> t-Butanol (TBA) EPA8260 5 ug/Kg ND 13-Oct-99 ND 70 102.9% 70 92.9% 100.0% :1.9% <br /> g,,,�,,,�,.,- �,�•.,.-.,®�..e - �,«., _ 20 i 10.0/o ° <br /> r�$ Benzene EPA 8260 5 uglKg ND 13-Oct-99 ND 20 110.0% 125.0°/ 3.2% <br /> p fY1 mem�.e �.�.-z� _ w««mm=�,a.•,m•ema.m®-�-n� '. __ <br /> Toluene EPA 8260 5 ug1Kg ND 13-Oct-99 ND 20 90.0% 20 110.0% 135.0% 5A% <br /> Ethyl Benzene EPA 8260 5 ug/Kg ND 13 Oct-99 ND 20 100.0% 20 125.0% 140.0% 2.8% <br /> Xylene,Tota! EPA 8.260 5 ug/Kg ND 13-Oct-99 ND 40 105.0% 40 137.5% 135.0% 0.5% <br /> ,rig/L = <br /> Milligrams per Liner=pprit DL'R=Detection Li,ui1 for flee Pu,pose'of R' RSD1-1iug. RSD represent relative lJercerrfdifferent(RPD)between duplicates spite of samples <br /> ug/L-mia'ogr a,tts per Lifer=ppb Exceptional sample matrices or hac,fereneces may resell in or Duplicate of Sample <br />,i higher defection tinrils AIS/MSD--measure of the percent recovery efficiencies within the matrix <br /> 4. C=Composile G=Grab <br /> a1:a <br /> ICS-measure of the percent recorer�>of the Lnbvra[ory Coariro!Spike <br /> RE'S TI U I7'TED,. <br /> Jonatlrau Hao v Le, Laborato►_p Director <br /> r •• EPA I7rvirori,nenfal Pr6tecrion Agency Alediad. Prrge 1 of I <br /> of <br /> SAI-Sla+rdardkrelhodforrxaminalion re .rr ,� � 1 � t. Suite A Stockton, CA 95204 Tel:: (209) 462-0892 Fax: (209) 462-7935 <br />