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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone: 925-798-1620 Fax: 925-798-1622 <br /> h-ttp://www.mcaampbell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Elkhorn Country Club Date Sampled: 04/27/01 <br /> 837 Shaw Road Date Received: 04/28/01 <br /> Stockton, CA 95215 Client Contact:Bill Little Date Extracted: 04/30-05/01/01 <br /> Client P.O: Date Analyzed: 04/30-05/01/01 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 66525 <br /> Reporting Limit <br /> Client ID IAS-3/ <br /> 04-27-01 <br /> Matrix W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(RIPE) ND 5.0 1.0 <br /> Ethyl tert-Butyl Ether(ETRE) ND 5.0 1.0 <br /> Methyl-tert Butyl Ether(MTBE) ND 5.0 1.0 <br /> tert-Amyl Methyl Ether(TAME) ND 5.0 1.0 <br /> -, tert-Butanol ND r25 5.0 <br /> Surrogate Recoveries <br /> Dibromofluoromethane 87 <br /> I <br /> Comments: <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I STLC 1 SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol.%sediment;0)sample diluted due to <br /> high organic content <br /> I <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br /> I <br />