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MAR-02-2005 17:18 CITY OF LODI 209 333 6710 P.22 <br /> GeaAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone(209)572-M Fax(209)572-0916 <br /> Report# R046-OB CERTIFICATE OF ANALYSIS Date: 2/23/05 <br /> Date Recd: 2/17/05 <br /> Thorpe Oil Date Started: 2/18/05 <br /> PO Box 357 Project: 230 West Elm St(Lodi) Date Completed:2/22/05 <br /> Lodi CA 95241 Date Sampled: 2/17/05 <br /> PO# Time: 1:15 pm <br /> Sample ID: Stockpile #6 Sampler : O.Sanchez(Geo) <br /> Lab ID: 8200177 <br /> Method RL Analyte Results Units <br /> 8260B 5.0 Benzene NO µ81A8 <br /> 5.0 Toluene ND <br /> 5.0 Ethyl Benzene ND <br /> 5.0 Total Xylenes ND <br /> 10 Methyl tert-butyl other(MTBE) NO <br /> 400 Ethanol ND <br /> 240 tort-Butanol NO <br /> 10 di-Isopropyl ether(DIPE) ND <br /> 10 Ethyl bert-butyl other(ETBE) NO <br /> 10 Cert-Amyl methyl ether(TANS) ND <br /> Sun-opte Amnt Spiked Amnt Rec. %Recovery OC Urnit% <br /> 1,2-Dichloroethane-4 20 19.9 99.5 66-133 <br /> 2-Bromo-l-chloropropane 20 16.8 84.0 63-139 <br /> 4-Bromofluorobawme 20 18.7 93.5 64-136 <br /> ado D'Onofri Donna Keller <br /> Chemist Certification #2585 Laboratory Director <br />