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MAR-02-2005 17: 17 CITY OF LODI 209 333 6710 P.18 <br /> GeoAnalyt'cal Laboratories, Inc. <br /> 1405 Kansas Avertue Modesto,CA 95351 Phone(209)572.0900 Fax(209)572-0916 <br /> Report R048-M CERTIFICATE OF ANALYSIS Date: 2/23/05 <br /> Date Rec'd: 2/17/05 <br /> Thorpe Oil Date Started: 2/18/05 <br /> FO Box 357 Project; 230 West Elm St(Lodi) Date Completed.2/18/05 <br /> Lodi CA 95241 <br /> Date Sampled; 2/17/05 <br /> PON Time: 1:11 pm <br /> Sample ID: Stockpile #4 Sampler: 0.Sanchez(Geo) <br /> Lab ID: 8200175 <br /> Method RL Ar& lit Results Unib <br /> 82608 5.0 Benzene NO µg/K5 <br /> 5.0 Toluene NO <br /> 5.0 Ethyl Benzene ND <br /> 5.0 Total Xylem NO <br /> 10 Methyl tert-butyl ether(MTBE) NO <br /> 400 Ethanol ND <br /> 200 tert-Bukanol NO <br /> 10 di-Isopropyl ether(DIPS) ND <br /> 10 Ethyl tert-butyl ether(ETBE) NO <br /> 10 tent-Amyl methyl ether(TAME) ND <br /> Surrogate Amnt Spired Amnt Ret. %Recovery QC Lirrdt% <br /> 1,2-Dichloroethane-4 20 24.7 123.5 66-133 <br /> 2-Bromo-i-chloropropane 20 20.5 1025 63-139 <br /> 4-Bromofluorobenzene 20 20.1 100.5 64-136 <br /> zariO4 D Onofno Donna Keller <br /> Chemist Certification #2585 Laboratory Director <br />