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GeoYunalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone(209)572-0900 Fax (209)572-0916 <br /> Report# R048-08 CERTIFICATE OF ANALYSIS Date: 2/23/05 <br /> Thorpe Oil Date Rec'd: 2/17/05 <br /> PO Box 357 Project: 230 West Elm St di Date Started: 2/18/05 <br /> Lodi CA 95241 Date Completed:2/22/05 <br /> Date Sampled: 2/17/05 <br /> PO# Time: 124 pm <br /> Sample ID: Hole#2 North End Sampler : O.Sanchez(Geo) <br /> Lab ID: 8200168 <br /> Method RL Analyte Results Units <br /> 8260B 5.0 Benzene ND µg/Kg <br /> 5.0 Toluene ND <br /> 5.0 Ethyl Benzene ND <br /> 5.0 Total Xylenes ND <br /> 1250 Methyl tert-butyl ether(MTBE) 18800 <br /> 400 Ethanol ND <br /> 200 tert-Butanol ND <br /> 10 di-Isopropyl ether(RIPE) ND <br /> 10 Ethyl tert-butyl ether(ETBE) ND <br /> 10 tert-Amyl methyl ether(TAME) ND <br /> Surrogate Amnt Spiked Amnt Rec. %Recovery QC Limit% <br /> 1,2-Dichloroethane-d4 2500 2480 99.2 66-133 <br /> 2-Bromo-l-chloropropane 2500 2170 86.8 63-139 <br /> 4-Bromofluorobenzene 2500 2390 95.6 64-136 <br /> iario�D'Onofri Donna Keller <br /> Chemist Certification #2585 Laboratory Director <br />