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f <br /> fr•r <br /> 03122196 <br /> QUALITY CONTROL REPORT DHS Certification #1400 <br /> Volatile Analyses <br /> Client: W.W. IRWIN Date Received: 03118196 <br /> 335 GROGAN AVE, SUITE A Date Started: : 03/19/95 <br /> MERCER, CA 95340 Date Complete: 03/20/96 <br /> `- ATTN: MIKE LUKSIC <br /> Lab Report#: H6031903 Lab Sample#s PH00314W-70 <br /> Linearity Check: <br /> BTEX Benzene 0.9990 TPH Gasoline 0.9999 <br /> Toluene 0.9986 TPH Diesel NIA <br /> f = Ethyl Benzene 0.9994 Motor Oil N/A <br /> Xylenes 0.9998 TRPH (419.1) NIA <br /> MTBE 0.9998 <br /> Std % Repesta biIity MTBE Benzene Toluene Eth Benz Xylenes <br /> f 3 BTEX 107 92 93 95 96 <br /> ' TPH Gasoline 99 TPH Diesel NIA <br /> TRPH (418.1) NIA TPH Motor Oil NIA <br /> Matrix Spike Recoveries MS MSD RPD <br /> MTBE 103.0 108.0 4.7 <br /> BTEX Benzene 91.0 101.0 10.4 <br /> Toluene 97.0 106.0 8.9 <br /> ` Ethyl Benzene 98.0 107.0. 8.8 <br /> -� Xylenes 97.0 107.0 9.8 <br /> TPH Gasoline 101.0 100.0 1.0 <br /> TPH Diesel N/A N/A ERR <br /> TRPH 418.1 N/A <br /> ==a <br /> Method Blank MTBE Benzene Toluene Eth Benz Xylenes <br /> F ! <br /> ccc- <br /> BTEX <2 ug/L [.3 uy/L <.3 ug/L <.3 uglL <.3 ug/L <br /> =-� TPH Gasoline <50 ug1L TPH Diesel/MO NIA TRPH(418.1) NIA <br /> Lab Control Sample% Recovery EPA Performance Acceptance Range <br /> BTEX Benzene 104 37.0 - 151.0 <br /> ' Tol uene 106 47.0 - 150.0 <br /> Ethyl Benz 107 36.9 - 162.0 <br /> - Xylenes 111 42.7 - 137.9 <br /> TPH Gasoline 104 35.0 - 130.1 <br /> .f, TPH Diesel NIA 45.1 - 135.2 <br /> TRPH (418.1) NIA NIA <br /> j= Gloria Poling, Lab Director 3 <br />