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1534 Willow Pass Road Pittsburg,CA 94565-1701 <br /> McCampbell Analytical, Inc. Toll Free Telephone:(877)252-9262/Fax:(925)252-9269 <br /> "When Quality Counts" httpl/w .mccampbeff.com/E-mail:main@=campbeu.com <br /> Quality Control Report <br /> Client: Safety-Kleen Corporation WorkOrder: 1809621 <br /> Date Prepared: 9/20/18 BatchID: 165281 <br /> Date Analyzed: 9/20/18 Extraction Method: SW5030B <br /> Instrument: GC16 Analytical Method: SW8260B <br /> Matrix: Water Unit: µg/L <br /> Project: 1;Kia Country Sump Water Sample ID: MB/LCS/LCSD-165281 <br /> QC Summary Report for SW8260B <br /> Analyte LCS LCSD SPK LCS LCSD LCS/LCSD RPD RPD <br /> Result Result Val %REC %REC Limits Limit <br /> cis-1,3-Dichloropropene 10.4 10.7 10 104 107 58-136 2.78 20 <br /> trans-1,3-Dichloropropene 10.4 10.6 10 104 106 66-119 1.87 20 <br /> Diisopropyl ether(DIPE) 11.3 11.6 10 113 116 66-123 2.24 20 <br /> Ethylbenzene 9.60 9.76 10 96 98 71-125 1.58 20 <br /> Ethyl tert-butyl ether(ETRE) 11.3 11.6 10 113 116 67-122 2.25 20 <br /> Freon 113 10.2 10.3 10 102 103 68-132 0.940 20 <br /> Hexachlorobutadiene 10.8 10.9 10 108 109 56-155 0.557 20 <br /> Hexachloroethane 9.47 9.52 10 95 95 61-129 0 20 <br /> 2-Hexanone 9.78 9.98 10 98 100 51-115 2.06 20 <br /> Isopropylbenzene 9.57 9.69 10 96 97 66-134 1.22 20 <br /> 4-Isopropyl toluene 9.72 9.88 10 97 99 70-136 1.69 20 <br /> Methyl-t-butyl ether(MTBE) 11.3 11.5 10 113 115 64118 1.75 20 <br /> Methylene chloride 10.5 10.4 10 105 104 62-121 0.351 20 <br /> 4-Methyl-2-pentanone(MIRK) 10.6 10.6 10 106 106 51-115 0 20 <br /> Naphthalene 10.3 10.7 10 103 107 55-137 4.01 20 <br /> n-Propyl benzene 10.7 10.8 10 107 108 63-140 1.24 20 <br /> Styrene 10.4 10.6 10 104 106 62-133 2.03 20 <br /> 1,1,1,2-Tetrachloroethane 9.82 10.2 10 98 103 69-128 4.28 20 <br /> 1,1,2,2-Tetrachloroethane 11.1 11.2 10 111 112 60-118 0.263 20 <br /> Tetrachloroethene 10.0 10.4 10 100 103 63-136 3.36 20 <br /> Toluene 10.0 10.1 10 101 101 67-124 0 20 <br /> 1,2,3-Trichlorobenzene 11.4 12.1 10 114 121 57-145 6.13 20 <br /> 1,2,4-Trichlorobenzene 12.0 12.3 10 120 123 60-144 2.44 20 <br /> 1,1,1-Trichloroethane 10.7 10.8 10 107 108 70-133 1.11 20 <br /> 1,1,2-Trichloroethane 10.2 10.5 10 102 105 65-125 3.08 20 <br /> Trichloroethene 11.0 11.4 10 110 114 67-133 2.94 20 <br /> Trichlorofluoromethane 9.45 9.57 10 94 96 59-145 1.30 20 <br /> 1,2,3-Trich I oropropane 9.78 9.54 10 98 95 65-115 2.48 20 <br /> 1,2,4-Trimethylbenzene 10.1 10.2 10 101 102 67-136 0.717 20 <br /> 1,3,5-Trimethylbenzene 10.0 10.2 10 100 102 68-135 1.47 20 <br /> Vinyl Chloride 9.38 8.93 10 94 89 53-146 5.00 20 <br /> m,p-Xylene 20.0 20.5 20 100 102 66-129 1.98,F2 0 <br /> o-Xylene 10.0 10.1 10 100 101 71-128 1.23,F2 0 <br /> Xylenes,Total 30.1 30.6 30 100 102 68-128 1.73 20 <br /> (Cont.) <br /> CA ELAP 1644•NELAP 4033ORELAP <br /> Page 12 of 20 <br />