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QC Report Matrix Spike/Matrix Spike Duplicate Report Number 31402 Date 02/25/2003 Protect Name E. 11 T ST. (68), TRACY Project Number Duplicate Duplicate Spiked Spike Spiked Spiked Spiked Spiked Sample Relative Spiked Sample Spike Dup Spiked Sam le Sample Sample Relative Percent Percent Parameter Sam le Value Level Level Value Value Units Methods Anal zed Recov t Recon t ©cent Remit v Limit PH as Diesel 31395-01 <1 0 200 200 21 8 198 mg/Kg M EPA 8015 2/13/03 109 988 986- 60-140 25 TPM as Diesel Blank <50 1000 1000 851 713 ug/L M EPA 8015 2113103 851 713 176 70-130 25 TPH as Diesel 31505-13 <1 0 200 200 167 21 7 mg/Kg M EPA 8015 2121103 834 108 260 60-140 25 Benkene 31460-01 <0 0050 00395 00394 00394 00396 mg/K9 EPA 8260B 2113103 998 100 0 600 70-130 25 Toluene 31460-01 <0 0050 00395 00394 00381 00383 mg/Kg EPA 82606 2113/03 964 970 0 620 70-130 25 Tert-Butanol 31460-01 <0 0050 0 198 0 197 0 180 0 182 m91K9 EPA 82608 2/13103 91 1 921 1 16 70-130 25 Methyl-t-Butyl Ether 31460-01 <0 0050 00395 00394 00366 00369 mg/Kg EPA 8260B 2/13/03 927 935 0 913 70-130 25 Benzene 31402-13 <0 50 19 9 198 188 187 ug/L EPA 8260B 2/15103 94 3 942 0106 70-130 25 Toluene 31402-13 <0 50 199 198 193 193 ug/L EPA 8260B 2115/03 971 972 00515 70-130 25 Tert-Bulanol 31402-13 <5 0 995 992 94 8 95 4 ug/L EPA 82606 2115103 953 961 0 872 70-130 25 Methyl-t-Butyl Ether 31402-13 <0 50 199 198 190 192 ug/L EPA 8260B 2115/03 957 96 7 104 70-130 25 Benzene 31505-20 <0 0050 00397 00398 00405 00392 mg/Kg EPA 8260E 2117103 102 985 356 70-130 25 Toluene 31505-20 <0 0050 00397 00398 00386 00373 mg/Kg EPA 8260B 2/17/03 97 4 93 9 3 61 70-130 25 Tert-Butanol 31505-20 <0 0050 0198 0199 0 182 0 178 mg/Kg EPA 8260E 2117103 919 893 2 92 70-130 25 Methyl-t-Butyl Ether 31505-20 <0 0050 00397 00398 00340 00325 mg/Kg EPA 8260B 2/17/03 856 818 463 70-130 25 KIFF ANALYTICAL, LLC Approved By J I Kiff 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800