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110 2nd Avenue South, #D7, Pacheco, CA 94553-5560 <br />124 1 McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />lin //www mccamobell com E-mail main@mccampbell com <br />Advanced GeoEnvironmental Client Project ID Tracy Dinner Date Sampled 04/26/01 <br />837 Shaw Road Date Received 04/26/01 <br />Stockton, CA 95215 Client Contact William Little Date Extracted 04/27/01 <br />Client P O Date Analyzed 04/27/01 <br />Seven Oxygenated Volatile Organics By GC/MS <br />EPA method 8260 modified <br />Lab 1D <br />66180 <br />66181 <br />66182 66183 <br />ClientlD <br />MWI / <br />042501 <br />MW2 / <br />042501 <br />MW3 / MW4 / <br />042501 042501 <br />Reporting Limit <br />Matrix <br />W <br />W <br />W W <br />S W <br />Compound <br />Concentration* <br />ug/kg ug/L <br />Di -isopropyl Ether (RIPE) <br />ND ND<2 5 <br />ND<2 5 <br />ND <br />50 10 <br />Ethyl tert-Butyl Ether (ETBE) <br />ND ND<2 5 <br />ND<2 5 <br />ND <br />50 10 <br />Methyl tert-Butyl Ether (MTBE) <br />ND ND<2 5 <br />ND<2 5 <br />ND <br />50 10 <br />tert-Amyl Methyl Ether (TAME) <br />ND ND<2 5 <br />ND<2 5 <br />ND <br />5 0 10 <br />tert-Butanol <br />ND ND<13 <br />ND<13 <br />ND <br />25 50 <br />Methanol <br />ND ND<1300 <br />ND<I300 <br />1000 500 <br />Ethanol <br />ND ND<130 <br />ND<130 <br />AND <br />250 50 <br />Dibromofluoromethane <br />Surrogate Recoveries (%) <br />94 93 95 96 <br />Comments I I J,h I ),h I I <br />* water samples are reported to ug/L, soil and sludge samples in ug/kg, wipes in ug/wipe and all TCL? / STLC / SPLP extracts in ug/L <br />ND means not detected above the reporting ]mut, N/A means surrogate not applicable to this analysis <br />(h) lighter than water immiscible sheen is present, (i) liquid sample that contains greater than --5 vol % sediment, 0) sample diluted due to <br />high organic content <br />DHS Certification No 1644 <br />J_ Edward Hanulton, Lab Director <br />