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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3 <br />Job Number: C17729 <br />Account: GEAICAO Giles Engineering Associates, Inc. <br />Project: 239 West 11th Street - Tracy, CA <br />Sample <br />File ID <br />DF <br />Analyzed <br />By <br />Prep Date <br />Prep Batch <br />Analytical Batch <br />C177294MS <br />M27146.D <br />1 <br />09/02/11 <br />XB <br />n/a <br />n/a <br />VM861 <br />C17729-4MSD <br />M27147.1) <br />1 <br />09/02/11 <br />XB <br />n/a <br />n/a <br />VM861 <br />C17729-4 <br />M27133.1) <br />1 <br />09/02/11 <br />XB <br />n/a <br />n/a <br />VM861 <br />The QC reported here applies to the following samples: Method: SW846 8260B <br />C17729-1, C17729-2, C17729-3, C17729-4, C17729-5 <br />ME 40 of 50 <br />M ACGUTEE3-G <br />C17729 <br />C177294 <br />Spike <br />MS <br />MS <br />MSD <br />MSD <br />Limits <br />CAS No. <br />Compound <br />ug/kg Q <br />ug/kg <br />ug/kg <br />% <br />ug/kg <br />% <br />RPD <br />Rec/RPD <br />67-64-1 <br />Acetone <br />ND <br />159 <br />210 <br />132* a <br />219 <br />137* a <br />4 <br />60-130/30 <br />71-43-2 <br />Benzene <br />ND <br />39.7 <br />41.5 <br />105 <br />41.5 <br />104 <br />0 <br />60-130/30 <br />108-86-1 <br />Bromobenzene <br />ND <br />39.7 <br />38.0 <br />96 <br />37.2 <br />93 <br />2 <br />60-130/30 <br />74-97-5 <br />Bromocldaromethane <br />ND <br />39.7 <br />43.8 <br />110 <br />44.4 <br />111 <br />1 <br />60-130/30 <br />75-27-4 <br />Bromodichloromethane <br />ND <br />39.7 <br />42.8 <br />108 <br />41.6 <br />104 <br />3 <br />60-130/30 <br />75-25-2 <br />Bromoform <br />ND <br />39.7 <br />40.6 <br />102 <br />39.9 <br />100 <br />2 <br />60-130/30 <br />104-51-8 <br />n-Butylbenzene <br />ND <br />39.7 <br />41.7 <br />105 <br />40.4 <br />101 <br />3 <br />60-130/30 <br />135-98-8 <br />sec-Bulylbenzene <br />ND <br />39.7 <br />40.8 <br />103 <br />40.3 <br />101 <br />1 <br />60-130/30 <br />98-06-6 <br />tert-Butylbenzene <br />ND <br />39.7 <br />39.3 <br />99 <br />38.6 <br />97 <br />2 <br />60-130/30 <br />108-90-7 <br />Chlorobenzene <br />ND <br />39.7 <br />37.8 <br />95 <br />37.4 <br />94 <br />1 <br />60-130/30 <br />75-00-3 <br />Chloroethane <br />ND <br />39.7 <br />45.3 <br />114 <br />45.9 <br />115 <br />1 <br />60-130/30 <br />67-66-3 <br />Chloroform <br />ND <br />39.7 <br />46.2 <br />116 <br />46.3 <br />116 <br />0 <br />60-130/30 <br />95-49-8 <br />o-Chlorotoluene <br />ND <br />39.7 <br />40.9 <br />103 <br />39.9 <br />100 <br />2 <br />60-130/30 <br />106-43-4 <br />p-Chlorotoluene <br />ND <br />39.7 <br />42.3 <br />107 <br />41.6 <br />104 <br />2 <br />60-130/30 <br />56-23-5 <br />Carbon tetrachloride <br />ND <br />39.7 <br />40.8 <br />103 <br />40.4 <br />101 <br />1 <br />60-130/30 <br />75-34-3 <br />1,1-Dichloroethane <br />ND <br />39.7 <br />45.8 <br />115 <br />46.4 <br />116 <br />1 <br />60-130/30 <br />75-35-4 <br />1,1-Dichloroethylene <br />ND <br />39.7 <br />42.0 <br />106 <br />42.4 <br />106 <br />1 <br />60-130/30 <br />563-58-6 <br />1,1-Dichloropropene <br />ND <br />39.7 <br />42.8 <br />108 <br />42.5 <br />107 <br />1 <br />60-130/30 <br />96-12-8 <br />1,2-Dibromo-3-chloropropane <br />ND <br />39.7 <br />52.9 <br />133* a <br />54.7 <br />137* a <br />3 <br />60-130/30 <br />106-93-4 <br />1,2-Dibromoethane <br />ND <br />39.7 <br />42.8 <br />108 <br />42.5 <br />107 <br />1 <br />60-130/30 <br />107-06-2 <br />1,2-Dichloroethane <br />ND <br />39.7 <br />46.4 <br />117 <br />45.6 <br />114 <br />2 <br />60-130/30 <br />78-87-5 <br />1,2-Dichloropropane <br />ND <br />39.7 <br />42.6 <br />107 <br />43.3 <br />109 <br />2 <br />60-130/30 <br />142-28-9 <br />1,3-Dichloropropane <br />ND <br />39.7 <br />44.3 <br />112 <br />43.6 <br />109 <br />2 <br />60-130/30 <br />108-20-3 <br />Di -Isopropyl ether <br />ND <br />39.7 <br />43.6 <br />110 <br />44.3 <br />111 <br />2 <br />60-130/30 <br />594-20-7 <br />2,2-Dichloropropane <br />ND <br />39.7 <br />47.1 <br />119 <br />47.2 <br />118 <br />0 <br />60-130/30 <br />124-48-1 <br />Dibromochloromethane <br />ND <br />39.7 <br />39.1 <br />99 <br />38.6 <br />97 <br />1 <br />60-130/30 <br />75-71-8 <br />Dichlorodifluoromethane <br />ND <br />39.7 <br />34.3 <br />86 <br />34.0 <br />85 <br />1 <br />60-130/30 <br />156-59-2 <br />cis-1,2-Dichloroethylene <br />ND <br />39.7 <br />43.7 <br />110 <br />44.3 <br />111 <br />1 <br />60-130/30 <br />10061-01-5 <br />cis-1,3-Dichloropropene <br />ND <br />39.7 <br />44.0 <br />111 <br />44.1 <br />111 <br />0 <br />60-130/30 <br />541-73-1 <br />no -Dichlorobenzene <br />ND <br />39.7 <br />37.4 <br />94 <br />36.0 <br />90 <br />4 <br />60-130/30 <br />95-50-1 <br />o -Dichlorobenzene <br />ND <br />39.7 <br />38.6 <br />97 <br />38.3 <br />96 <br />1 <br />60-130/30 <br />106-46-7 <br />p -Dichlorobenzene <br />ND <br />39.7 <br />38.1 <br />96 <br />37.2 <br />93 <br />2 <br />60-130/30 <br />156-60-5 <br />trans-1,2-Dichloroethylene <br />ND <br />39.7 <br />42.3 <br />107 <br />42.9 <br />108 <br />1 <br />60-130/30 <br />10061-02-6 <br />trans-1,3-Dichloropropene <br />ND <br />39.7 <br />40.4 <br />102 <br />39.9 <br />100 <br />1 <br />60-130/30 <br />100-41-4 <br />Ethylbenzene <br />ND <br />39.7 <br />39.8 <br />100 <br />39.3 <br />99 <br />1 <br />60-130/30 <br />637-92-3 <br />Ethyl tert-Butyl Ether <br />ND <br />39.7 <br />51.3 <br />129 <br />52.4 <br />132* a <br />2 <br />60-130/30 <br />ME 40 of 50 <br />M ACGUTEE3-G <br />C17729 <br />