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Matrix Spike/Matrix Spike Duplicate Summary <br />Job Number: C17729 <br />Account: GEAICAO Giles Engineering Associates, Inc. <br />Project: 239 West 11th Street - Tracy, CA <br />Page 3 of 3 <br />Sample <br />File ID <br />DF <br />Analyzed <br />By <br />Prep Date <br />Prep Batch <br />Analytical Batch <br />C177294MS <br />M27146.D <br />1 <br />09/02/11 <br />XB <br />n/a <br />n/a <br />VM861 <br />C17729-4MSD <br />M27147.D <br />1 <br />09/02/11 <br />XB <br />n/a <br />n/a <br />VM861 <br />C17729-4 <br />M27133.D <br />1 <br />09/02/11 <br />XB <br />n/a <br />n/a <br />VM861 <br />The QC reported here applies to the following samples: <br />Method: SW846 8260B <br />C17729-1, C17729-2, C17729-3, C17729-4, C17729-5 <br />CAS No. Surrogate Recoveries MS MSD <br />C17729-4 <br />Limits <br />2037-26-5 Toluene -D8 98% 98% <br />101% <br />60-130% <br />460-00-4 4-Bromofluorobenzene 102% 102% <br />98% <br />60-130% <br />(a) Outside laboratory control limits. <br />ME 42 of 50 <br />N ACCUTEST. <br />C17729 <br />