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0 0 <br />Blank Spike/Blank Spike Duplicate Summary Page 2 of 3 <br />Job Number: C17728 <br />Account: GEAICAO Giles Engineering Associates, Inc. <br />Project: 239 West 11th Street - Tracy, CA <br />Sample <br />File ID <br />DF <br />Analyzed <br />By <br />Prep Date <br />Prep Batch <br />Analytical Batch <br />VL321-BS <br />L10247.1) <br />1 <br />09/02/11 <br />TF <br />n/a <br />n/a <br />VL321 <br />VL321-BSD <br />L10248.1) <br />1 <br />09/02/11 <br />TF <br />n/a <br />n/a <br />VL321 <br />The QC reported here applies to the following samples: Method: SW846 8260B <br />C17728-1, C17728-2, C17728-3, C17728-4 <br />ffin 25 of 29 <br />N AGCUTE8T. <br />C17728 Ln O...-1- <br />Spike <br />BSP <br />BSP <br />BSD <br />BSD <br />Limits <br />CAS No. <br />Compound <br />ug/1 <br />ug/1 <br />% <br />ug/I <br />% <br />RPD <br />Roe/RPD <br />591-78-6 <br />2-Hexanone <br />80 <br />94.9 <br />119 <br />93.8 <br />117 <br />1 <br />60-130/30 <br />87-68-3 <br />Hexachlorobutadiene <br />20 <br />20.0 <br />100 <br />20.2 <br />101 <br />1 <br />60-130/30 <br />98-82-8 <br />Isopropylbenzene <br />20 <br />16.2 <br />81 <br />16.1 <br />81 <br />1 <br />60-130/30 <br />99-87-6 <br />p-Isopropyltoluene <br />20 <br />17.3 <br />87 <br />17.2 <br />86 <br />1 <br />60-130/30 <br />108-10-1 <br />4-Methyl-2-pentanone <br />80 <br />77.2 <br />97 <br />76.6 <br />96 <br />1 <br />60-130/30 <br />74-83-9 <br />Methyl bromide <br />20 <br />20.9 <br />105 <br />20.4 <br />102 <br />2 <br />60-130/30 <br />74-87-3 <br />Methyl chloride <br />20 <br />19.2 <br />96 <br />19.3 <br />97 <br />1 <br />60-130/30 <br />74-95-3 <br />Methylene bromide <br />20 <br />19.3 <br />97 <br />19.3 <br />97 <br />0 <br />60-130/30 <br />75-09-2 <br />Methylene chloride <br />20 <br />17.2 <br />86 <br />17.3 <br />87 <br />1 <br />60-130/30 <br />78-93-3 <br />Methyl ethyl ketone <br />80 <br />86.6 <br />108 <br />86.0 <br />108 <br />1 <br />60-130/30 <br />1634-04-4 <br />Methyl Tert Butyl Ether <br />20 <br />18.1 <br />91 <br />18.1 <br />91 <br />0 <br />60-130/30 <br />91-20-3 <br />Naphthalene <br />20 <br />17.4 <br />87 <br />18.1 <br />91 <br />4 <br />60-130/30 <br />103-65-1 <br />n-Propylbenzene <br />20 <br />18.0 <br />90 <br />18.0 <br />90 <br />0 <br />60-130/30 <br />100-42-5 <br />Styrene <br />20 <br />20.0 <br />100 <br />19.8 <br />99 <br />1 <br />60-130/30 <br />994-05-8 <br />Tert-Amyl Methyl Ether <br />20 <br />18.2 <br />91 <br />18.2 <br />91 <br />0 <br />60-130/30 <br />75-65-0 <br />Tert-Butyl Alcohol <br />100 <br />79.1 <br />79 <br />75.5 <br />76 <br />5 <br />60-130/30 <br />630-20-6 <br />1,1,1,2 -Tetrachloroethane <br />20 <br />20.6 <br />103 <br />20.4 <br />102 <br />1 <br />60-130/30 <br />71-55-6 <br />1,1,1 -Trichloroethane <br />20 <br />17.0 <br />85 <br />16.6 <br />83 <br />2 <br />60-130/30 <br />79-34-5 <br />1,1,2,2 -Tetrachloroethane <br />20 <br />20.0 <br />100 <br />19.8 <br />99 <br />1 <br />60-130/30 <br />79-00-5 <br />1,1,2 -Trichloroethane <br />20 <br />20.0 <br />100 <br />20.1 <br />101 <br />0 <br />60-130/30 <br />87-61-6 <br />1, 2,3-Trichl orobenzene <br />20 <br />18.8 <br />94 <br />19.2 <br />96 <br />2 <br />60-130/30 <br />96-18-4 <br />1, 2, 3-Trichl oropropane <br />20 <br />18.6 <br />93 <br />18.9 <br />95 <br />2 <br />60-130/30 <br />120-82-1 <br />1,2,4-Trichlorobenzene <br />20 <br />18.1 <br />91 <br />18.5 <br />93 <br />2 <br />60-130/30 <br />95-63-6 <br />1,2,4-Trimethylbenzene <br />20 <br />18.7 <br />94 <br />18.9 <br />95 <br />1 <br />60-130/30 <br />108-67-8 <br />1, 3,5 -Trimethylbenzene <br />20 <br />19.2 <br />96 <br />19.2 <br />96 <br />0 <br />60-130/30 <br />127-18-4 <br />Tetrachloroethylene <br />20 <br />15.8 <br />79 <br />16.6 <br />83 <br />5 <br />60-130/30 <br />108-88-3 <br />Toluene <br />20 <br />18.3 <br />92 <br />18.2 <br />91 <br />1 <br />60-130/30 <br />79-01-6 <br />Trichloroethylene <br />20 <br />17.5 <br />88 <br />17.5 <br />88 <br />0 <br />60-130/30 <br />75-69-4 <br />Trichlorofluoromethane <br />20 <br />19.3 <br />97 <br />18.5 <br />93 <br />4 <br />60-130/30 <br />75-01-4 <br />Vinyl chloride <br />20 <br />24.0 <br />120 <br />23.1 <br />116 <br />4 <br />60-130/30 <br />1330-20-7 <br />Xylene (total) <br />60 <br />56.2 <br />94 <br />56.0 <br />93 <br />0 <br />60-130/30 <br />CAS No. <br />Surrogate Recoveries <br />BSP <br />BSD <br />Limits <br />1868-53-7 <br />Dibromofluoromethane <br />99% <br />98% <br />60-130% <br />ffin 25 of 29 <br />N AGCUTE8T. <br />C17728 Ln O...-1- <br />